C₁₄H₁₃BrF₄N₂O

Base Information Edit

Chemical Name:C₁₄H₁₃BrF₄N₂O
CAS No.:1352420-03-1
Molecular Formula:C₁₄H₁₃BrF₄N₂O
Molecular Weight:381.168
Hs Code.:
Mol file:1352420-03-1.mol

C<sub>14</sub>H<sub>13</sub>BrF<sub>4</sub>N<sub>2</sub>O

Synonyms:C₁₄H₁₃BrF₄N₂O

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Chemical Property of C₁₄H₁₃BrF₄N₂O Edit

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Technology Process of C₁₄H₁₃BrF₄N₂O

There total 12 articles about C₁₄H₁₃BrF₄N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1352420-02-0
C₁₄H₁₂BrF₄NOS

: 1352420-04-2
C₁₄H₁₃BrF₄N₂O

: 1352420-03-1
C₁₄H₁₃BrF₄N₂O

Guidance literature:: With ammonium hydroxide; ammonia; In quinoline; water; at 140 ℃; for 1h; Microwave irradiation;

Reference yield:

: 62123-80-2
ethyl 2-(3-bromo-phenyl)-2-oxo-acetate

: 1352420-04-2
C₁₄H₁₃BrF₄N₂O

: 1352420-03-1
C₁₄H₁₃BrF₄N₂O

Guidance literature:: Multi-step reaction with 10 steps

1.1: titanium(IV) tetraethanolate / n-heptane / 24 h / 80 °C

2.1: dichloromethane / 0.67 h / -40 °C

3.1: sodium hydroxide; water / methanol / 4 h / Reflux

4.1: hydrogenchloride / 1,4-dioxane; water / 0.5 h / 20 °C

5.1: sodium hydroxide / water; tetrahydrofuran / 15 °C / pH 10 - 11

5.2: pH 2

6.1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 2 h / 8 °C

7.1: tetrabutylammonium triphenyldifluorosilicate / tetrahydrofuran / 2 h / 20 °C

8.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / 20 °C

9.1: tetraphosphorus decasulfide / tetrahydrofuran / 3 h / 20 - 70 °C

10.1: ammonium hydroxide; ammonia / water; quinoline / 1 h / 140 °C / Microwave irradiation

With hydrogenchloride; titanium(IV) tetraethanolate; ammonium hydroxide; tetraphosphorus decasulfide; diethylamino-sulfur trifluoride; ammonia; water; sodium hydrogencarbonate; tetrabutylammonium triphenyldifluorosilicate; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; quinoline; methanol; n-heptane; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1352419-96-5
C₁₅H₂₀BrNO₃S

: 1352420-04-2
C₁₄H₁₃BrF₄N₂O

: 1352420-03-1
C₁₄H₁₃BrF₄N₂O

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogenchloride / 1,4-dioxane; water / 0.5 h / 20 °C

2.1: sodium hydroxide / water; tetrahydrofuran / 15 °C / pH 10 - 11

2.2: pH 2

3.1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 2 h / 8 °C

4.1: tetrabutylammonium triphenyldifluorosilicate / tetrahydrofuran / 2 h / 20 °C

5.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / 20 °C

6.1: tetraphosphorus decasulfide / tetrahydrofuran / 3 h / 20 - 70 °C

7.1: ammonium hydroxide; ammonia / water; quinoline / 1 h / 140 °C / Microwave irradiation

With hydrogenchloride; ammonium hydroxide; tetraphosphorus decasulfide; diethylamino-sulfur trifluoride; ammonia; sodium hydrogencarbonate; tetrabutylammonium triphenyldifluorosilicate; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; quinoline; dichloromethane; water; N,N-dimethyl-formamide;