C₃₀H₅₂O₅Si₂

Base Information

Chemical Name:C₃₀H₅₂O₅Si₂
CAS No.:1392098-00-8
Molecular Formula:C₃₀H₅₂O₅Si₂
Molecular Weight:548.911
Hs Code.:

C<sub>30</sub>H<sub>52</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:C₃₀H₅₂O₅Si₂

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Chemical Property of C₃₀H₅₂O₅Si₂

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Technology Process of C₃₀H₅₂O₅Si₂

There total 6 articles about C₃₀H₅₂O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1392097-97-0
C₃₅H₆₀O₆Si₂

: 1392098-00-8
C₃₀H₅₂O₅Si₂

Guidance literature:: With diisobutylaluminium hydride; In hexane; dichloromethane; at -78 - 20 ℃; for 0.583333h; Inert atmosphere;
DOI:10.3762/bjoc.8.82

Reference yield:

: 5159-41-1
2-iodobenzyl alcohol

: 1392098-00-8
C₃₀H₅₂O₅Si₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / dichloromethane / 18 h / 20 °C

2.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium t-butanolate / toluene / Inert atmosphere

2.2: 20 h / 50 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.58 h / -78 - 20 °C / Inert atmosphere

With pyridine; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; diisobutylaluminium hydride; sodium t-butanolate; In hexane; dichloromethane; toluene;
DOI:10.3762/bjoc.8.82

Reference yield:

: 191593-14-3
4,6-O-di(tert-butyl)silanediyl-D-glucal

: 1392098-00-8
C₃₀H₅₂O₅Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 68 h / 20 - 60 °C / Inert atmosphere

2.1: tert.-butyl lithium / diethyl ether; pentane / 2 h / -78 - 0 °C / Inert atmosphere

2.2: 1 h / -78 - 20 °C / Inert atmosphere

3.1: [RhCl₂(p-cymene)]2; water / acetonitrile; benzene / 4 h / 20 °C

4.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium t-butanolate / toluene / Inert atmosphere

4.2: 20 h / 50 °C / Inert atmosphere

5.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.58 h / -78 - 20 °C / Inert atmosphere

With 1H-imidazole; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; [RhCl₂(p-cymene)]2; water; tert.-butyl lithium; diisobutylaluminium hydride; sodium t-butanolate; In diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; pentane; benzene;
DOI:10.3762/bjoc.8.82