6,12-bis(3,4-dimethoxyphenyl)-5,6,11,12-tetrahydroindolo[3,2-b]carbazole

Base Information

• Chemical Name: 6,12-bis(3,4-dimethoxyphenyl)-5,6,11,12-tetrahydroindolo[3,2-b]carbazole
• CAS No.: 1613810-39-1
• Molecular Formula: C₃₄H₃₀N₂O₄
• Molecular Weight: 530.623
• Mol file: 1613810-39-1.mol

Synonyms:6,12-bis(3,4-dimethoxyphenyl)-5,6,11,12-tetrahydroindolo[3,2-b]carbazole

Chemical Property of 6,12-bis(3,4-dimethoxyphenyl)-5,6,11,12-tetrahydroindolo[3,2-b]carbazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6,12-bis(3,4-dimethoxyphenyl)-5,6,11,12-tetrahydroindolo[3,2-b]carbazole

There total 1 articles about 6,12-bis(3,4-dimethoxyphenyl)-5,6,11,12-tetrahydroindolo[3,2-b]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

indole (120-72-9) + 3,4-dimethoxy-benzaldehyde (120-14-9) → 6,12-bis(3,4-dimethoxyphenyl)-5,6,11,12-tetrahydroindolo[3,2-b]carbazole (1613810-39-1)

Guidance literature:

With tetrafluoroboric acid; tetra-(n-butyl)ammonium iodide; In water; acetonitrile; at 15 - 20 ℃; for 4h;

DOI:10.1016/j.tet.2014.04.093

Reference yield: 56.0%

6,12-bis(3,4-dimethoxyphenyl)-5,6,11,12-tetrahydroindolo[3,2-b]carbazole (1613810-39-1) → 6,12-bis(3,4-dimethoxyphenyl)-5,11-dihydroindolo[3,2-b]carbazole

Guidance literature:

With iodine; In acetone; for 14h; Reflux;

DOI:10.1002/jhet.4153

Reference yield:

1-Bromoheptane (629-04-9) + 6,12-bis(3,4-dimethoxyphenyl)-5,6,11,12-tetrahydroindolo[3,2-b]carbazole (1613810-39-1) → 6,12-bis(3,4-dimethoxyphenyl)-5,11-diheptyl-5,6,11,12-tetrahydroindolo[3,2-b]carbazole (1613810-45-9)

Guidance literature:

6,12-bis(3,4-dimethoxyphenyl)-5,6,11,12-tetrahydroindolo[3,2-b]carbazole; With sodium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;

1-Bromoheptane; In N,N-dimethyl-formamide; for 15h; Inert atmosphere;

DOI:10.1016/j.tet.2014.04.093

upstream raw materials:

indole

3,4-dimethoxy-benzaldehyde

Downstream raw materials:

6,12-bis(3,4-dimethoxyphenyl)-5,11-diheptyl-5,6,11,12-tetrahydroindolo[3,2-b]carbazole