N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 6-O-acetyl-2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl-(1->4)-2-azido-3-O-benzyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside

Base Information

Chemical Name:N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 6-O-acetyl-2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl-(1->4)-2-azido-3-O-benzyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside
CAS No.:1334709-69-1
Molecular Formula:C₉₄H₁₀₈Cl₃N₇O₂₇SSi
Molecular Weight:1934.43
Hs Code.:

N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 6-O-acetyl-2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl-(1->4)-2-azido-3-O-benzyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside

Synonyms:N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 6-O-acetyl-2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl-(1->4)-2-azido-3-O-benzyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside

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Chemical Property of N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 6-O-acetyl-2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl-(1->4)-2-azido-3-O-benzyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside

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Technology Process of N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 6-O-acetyl-2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl-(1->4)-2-azido-3-O-benzyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside

There total 1 articles about N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 6-O-acetyl-2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl-(1->4)-2-azido-3-O-benzyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1334709-61-3
N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 6-O-acetyl-2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-6-O-levulinoyl-β-D-glucopyranosyl-(1->4)-2-azido-3-O-benzyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-6-O-levulinoyl-β-D-glucopyranoside

: 1334709-69-1
N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 6-O-acetyl-2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl-(1->4)-2-azido-3-O-benzyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside

Guidance literature:: With pyridine; hydrazine hydrate; acetic acid; at 0 ℃; for 6h; Inert atmosphere;
DOI:10.1002/chem.201101108

Reference yield:

: 1334709-69-1
N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 6-O-acetyl-2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl-(1->4)-2-azido-3-O-benzyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside

: C₉₄H₁₀₄Cl₃N₇O₂₉SSi

Guidance literature:: N-(benzyl)-benzyloxycarbonyl-3-aminopropyl 6-O-acetyl-2-azido-3-O-benzyl-4-O-tert-butyldimethylsilyl-2-deoxy-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl-(1->4)-2-azido-3-O-benzyl-2-deoxy-6-O-(2,2,2-trichloroethylsulfuryl)-α-D-glucopyranosyl-(1->4)-2-O-benzoyl-3-O-benzyl-β-D-glucopyranoside; With sodium hypochlorite solution; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutylammomium bromide; sodium hydrogencarbonate; sodium bromide; In dichloromethane; water; at 0 - 20 ℃; for 1h; Inert atmosphere;

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In tetrahydrofuran; dichloromethane; water; acetic acid; tert-butyl alcohol; at 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201101108