N-(tert-butoxycarbonyl)-N, N'-bis(mesitylenesulfonyl)-1,4-diaminobutane

Base Information

Chemical Name:N-(tert-butoxycarbonyl)-N, N'-bis(mesitylenesulfonyl)-1,4-diaminobutane
CAS No.:161452-10-4
Molecular Formula:C₂₇H₄₀N₂O₆S₂
Molecular Weight:552.756
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)-N, N'-bis(mesitylenesulfonyl)-1,4-diaminobutane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(tert-butoxycarbonyl)-N, N'-bis(mesitylenesulfonyl)-1,4-diaminobutane

Chemical Property:

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Technology Process of N-(tert-butoxycarbonyl)-N, N'-bis(mesitylenesulfonyl)-1,4-diaminobutane

There total 6 articles about N-(tert-butoxycarbonyl)-N, N'-bis(mesitylenesulfonyl)-1,4-diaminobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 773-64-8
2-mesitylenesulphonyl chloride

: 161452-09-1
N-(tert-butoxycarbonyl)-N-(4-aminobutyl)mesitylenesulfonamide

: 161452-10-4
N-(tert-butoxycarbonyl)-N, N'-bis(mesitylenesulfonyl)-1,4-diaminobutane

Guidance literature:: With sodium hydroxide; In dichloromethane; at 0 - 20 ℃; for 24h;
DOI:10.1021/jm00047a004

Reference yield:

: 21926-49-8
2,4,6-Trimethylbenzol-sulfonylisocyanat

: 161452-10-4
N-(tert-butoxycarbonyl)-N, N'-bis(mesitylenesulfonyl)-1,4-diaminobutane

Guidance literature:: Multi-step reaction with 4 steps

1: various solvent(s) / 8 h / Ambient temperature

2: 1.) NaI, NaH / 1.) DMF, 25 min, 2.) DMF, 70 deg C, 1 d

3: 100 percent / H₂, conc. NH₄OH / Raney Ni / methanol / 6 h / 50 - 55 Torr

4: 87 percent / 1N aq. NaOH / CH₂Cl₂ / 24 h / 0 - 20 °C

With ammonium hydroxide; sodium hydroxide; hydrogen; sodium hydride; sodium iodide; nickel; In methanol; dichloromethane;
DOI:10.1021/jm00047a004

Reference yield:

: 56830-76-3
(2,4,6-trimethylbenzenesulfonyl)carbamic acid tert-butyl ester

: 161452-10-4
N-(tert-butoxycarbonyl)-N, N'-bis(mesitylenesulfonyl)-1,4-diaminobutane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaI, NaH / 1.) DMF, 25 min, 2.) DMF, 70 deg C, 1 d

2: 100 percent / H₂, conc. NH₄OH / Raney Ni / methanol / 6 h / 50 - 55 Torr

3: 87 percent / 1N aq. NaOH / CH₂Cl₂ / 24 h / 0 - 20 °C

With ammonium hydroxide; sodium hydroxide; hydrogen; sodium hydride; sodium iodide; nickel; In methanol; dichloromethane;
DOI:10.1021/jm00047a004