C₃₄H₄₄O₄Si

Base Information

Chemical Name:C₃₄H₄₄O₄Si
CAS No.:1286242-05-4
Molecular Formula:C₃₄H₄₄O₄Si
Molecular Weight:544.806
Hs Code.:

C<sub>34</sub>H<sub>44</sub>O<sub>4</sub>Si

Synonyms:C₃₄H₄₄O₄Si

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Chemical Property of C₃₄H₄₄O₄Si

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Technology Process of C₃₄H₄₄O₄Si

There total 11 articles about C₃₄H₄₄O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1286242-03-2
C₃₅H₄₄O₅Si

: 1286242-05-4
C₃₄H₄₄O₄Si

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; at 0 ℃;
DOI:10.3987/COM-10-12106

Reference yield:

: 1286241-95-9
C₃₀H₄₈O₃Si₂

: 1286242-05-4
C₃₄H₄₄O₄Si

Guidance literature:: Multi-step reaction with 6 steps

1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -30 °C

2: Dess-Martin periodane / dichloromethane

3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran; water

4: trimethylaluminum / dichloromethane; water / -50 °C

5: toluene-4-sulfonic acid / benzene / Reflux

6: diisobutylaluminium hydride / tetrahydrofuran / 0 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate; trimethylaluminum; diisobutylaluminium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; water; benzene; 1: Katsuki-Sharpless epoxidation / 2: Dess-Martin oxidation / 2: Wittig reaction;
DOI:10.3987/COM-10-12106

Reference yield:

: 1286241-94-8
C₃₁H₄₈O₄Si₂

: 1286242-05-4
C₃₄H₄₄O₄Si

Guidance literature:: Multi-step reaction with 7 steps

1: diisobutylaluminium hydride / tetrahydrofuran / 0 °C

2: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -30 °C

3: Dess-Martin periodane / dichloromethane

4: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran; water

5: trimethylaluminum / dichloromethane; water / -50 °C

6: toluene-4-sulfonic acid / benzene / Reflux

7: diisobutylaluminium hydride / tetrahydrofuran / 0 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate; trimethylaluminum; diisobutylaluminium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; water; benzene; 2: Katsuki-Sharpless epoxidation / 3: Dess-Martin oxidation / 3: Wittig reaction;
DOI:10.3987/COM-10-12106