(2E,5S,6S,7R,8Z)-6,8-dimethyl-7,10-bis(triisopropylsiloxy)-1-(triphenylmethoxy)deca-2,8-dien-5-yl 1-azidocyclopropanecarboxylate

Base Information

Chemical Name:(2E,5S,6S,7R,8Z)-6,8-dimethyl-7,10-bis(triisopropylsiloxy)-1-(triphenylmethoxy)deca-2,8-dien-5-yl 1-azidocyclopropanecarboxylate
CAS No.:1071850-51-5
Molecular Formula:C₅₃H₇₉N₃O₅Si₂
Molecular Weight:894.398
Hs Code.:

Synonyms:(2E,5S,6S,7R,8Z)-6,8-dimethyl-7,10-bis(triisopropylsiloxy)-1-(triphenylmethoxy)deca-2,8-dien-5-yl 1-azidocyclopropanecarboxylate

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Chemical Property of (2E,5S,6S,7R,8Z)-6,8-dimethyl-7,10-bis(triisopropylsiloxy)-1-(triphenylmethoxy)deca-2,8-dien-5-yl 1-azidocyclopropanecarboxylate

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Technology Process of (2E,5S,6S,7R,8Z)-6,8-dimethyl-7,10-bis(triisopropylsiloxy)-1-(triphenylmethoxy)deca-2,8-dien-5-yl 1-azidocyclopropanecarboxylate

There total 1 articles about (2E,5S,6S,7R,8Z)-6,8-dimethyl-7,10-bis(triisopropylsiloxy)-1-(triphenylmethoxy)deca-2,8-dien-5-yl 1-azidocyclopropanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: C₄H₄ClN₃O

: 1071850-50-4
(2E,5S,6S,7R,8Z)-6,8-dimethyl-7,10-bis(triisopropylsiloxy)-1-(triphenylmethoxy)deca-2,8-dien-5-ol

: 1071850-51-5
(2E,5S,6S,7R,8Z)-6,8-dimethyl-7,10-bis(triisopropylsiloxy)-1-(triphenylmethoxy)deca-2,8-dien-5-yl 1-azidocyclopropanecarboxylate

Guidance literature:: With dmap; triethylamine; In dichloromethane; benzene; at 0 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1002/anie.200802079

Reference yield: 84.0%

: 1071850-51-5
(2E,5S,6S,7R,8Z)-6,8-dimethyl-7,10-bis(triisopropylsiloxy)-1-(triphenylmethoxy)deca-2,8-dien-5-yl 1-azidocyclopropanecarboxylate

: 1071850-53-7
(2E,5S,6S,7R,8Z)-10-hydroxy-6,8-dimethyl-7-(triisopropylsiloxy)-1-(triphenylmethoxy)deca-2,8-dien-5-yl 1-azidocyclopropanecarboxylate

Guidance literature:: With pyridine hydrofluoride; In tetrahydrofuran; at 0 - 23 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1002/anie.200802079