(+/-)-methyl 2-{[({3-[(methoxycarbonyl)methyl]phenyl}amino)sulfonyl]amino}-3(naphthalen-2-yl)propanoate

Base Information

Chemical Name:(+/-)-methyl 2-{[({3-[(methoxycarbonyl)methyl]phenyl}amino)sulfonyl]amino}-3(naphthalen-2-yl)propanoate
CAS No.:259794-48-4
Molecular Formula:C₂₃H₂₄N₂O₆S
Molecular Weight:456.519
Hs Code.:

Synonyms:(+/-)-methyl 2-{[({3-[(methoxycarbonyl)methyl]phenyl}amino)sulfonyl]amino}-3(naphthalen-2-yl)propanoate

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Chemical Property of (+/-)-methyl 2-{[({3-[(methoxycarbonyl)methyl]phenyl}amino)sulfonyl]amino}-3(naphthalen-2-yl)propanoate

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Technology Process of (+/-)-methyl 2-{[({3-[(methoxycarbonyl)methyl]phenyl}amino)sulfonyl]amino}-3(naphthalen-2-yl)propanoate

There total 3 articles about (+/-)-methyl 2-{[({3-[(methoxycarbonyl)methyl]phenyl}amino)sulfonyl]amino}-3(naphthalen-2-yl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 123929-73-7
(+/-)-3-(2-naphthyl)alanine methyl ester hydrochloride

: 259794-47-3
methyl 2-(3-{[(2-oxo-1,3-oxazolan-3-yl)sulfonyl]amino}phenyl)ethanoate

: 259794-48-4
(+/-)-methyl 2-{[({3-[(methoxycarbonyl)methyl]phenyl}amino)sulfonyl]amino}-3(naphthalen-2-yl)propanoate

Guidance literature:: With triethylamine; In acetonitrile; for 12h; Heating;
DOI:10.1002/(SICI)1522-2675(19991215)82:12<2432::AID-HLCA2432>3.0.CO;2-H

Reference yield:

: 52913-11-8
(3-amino-phenyl)-acetic acid methyl ester

: 259794-48-4
(+/-)-methyl 2-{[({3-[(methoxycarbonyl)methyl]phenyl}amino)sulfonyl]amino}-3(naphthalen-2-yl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / 12 h / 20 °C

2: 1.39 g / Et₃N / CH₂Cl₂ / 6 h / 20 °C

3: 90 percent / Et₃N / acetonitrile / 12 h / Heating

With triethylamine; In dichloromethane; acetonitrile; 1: Condensation / 2: Cyclization / 3: Substitution;
DOI:10.1002/(SICI)1522-2675(19991215)82:12<2432::AID-HLCA2432>3.0.CO;2-H

Reference yield:

: C₁₂H₁₅ClN₂O₆S

: 259794-48-4
(+/-)-methyl 2-{[({3-[(methoxycarbonyl)methyl]phenyl}amino)sulfonyl]amino}-3(naphthalen-2-yl)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.39 g / Et₃N / CH₂Cl₂ / 6 h / 20 °C

2: 90 percent / Et₃N / acetonitrile / 12 h / Heating

With triethylamine; In dichloromethane; acetonitrile; 1: Cyclization / 2: Substitution;
DOI:10.1002/(SICI)1522-2675(19991215)82:12<2432::AID-HLCA2432>3.0.CO;2-H