sinenside A

Base Information

• Chemical Name: sinenside A
• CAS No.: 1363339-37-0
• Molecular Formula: C₂₃H₂₆O₁₁
• Molecular Weight: 478.453

Synonyms:sinenside A

Chemical Property of sinenside A

Chemical Property:

Purity/Quality:

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Technology Process of sinenside A

There total 3 articles about sinenside A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

C72H68O11 → sinenside A (1363339-37-0)

Guidance literature:

With 20% palladium hydroxide-activated charcoal; hydrogen; In ethyl acetate; at 20 ℃; under 750.075 Torr;

DOI:10.1021/acs.orglett.5b00505

Reference yield:

C73H72O11 → sinenside A (1363339-37-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 2,6-dimethylpyridine; osmium(VIII) oxide; sodium periodate / water; toluene; 1,4-dioxane / 5 h / 0 - 20 °C

2: camphor-10-sulfonic acid / benzene / 1 h / 20 °C

3: 20% palladium hydroxide-activated charcoal; hydrogen / ethyl acetate / 20 °C / 750.08 Torr

With 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; 20% palladium hydroxide-activated charcoal; camphor-10-sulfonic acid; hydrogen; In 1,4-dioxane; water; ethyl acetate; toluene; benzene;

DOI:10.1021/acs.orglett.5b00505

Reference yield:

C72H70O12 → sinenside A (1363339-37-0)

Guidance literature:

Multi-step reaction with 2 steps

1: camphor-10-sulfonic acid / benzene / 1 h / 20 °C

2: 20% palladium hydroxide-activated charcoal; hydrogen / ethyl acetate / 20 °C / 750.08 Torr

With 20% palladium hydroxide-activated charcoal; camphor-10-sulfonic acid; hydrogen; In ethyl acetate; benzene;

DOI:10.1021/acs.orglett.5b00505

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