5-(2-Hydroxy-phenyl)-3-(2-oxo-2-phenothiazin-10-yl-ethyl)-2-phenyl-3H-tetrazol-2-ium; chloride

Base Information

Chemical Name:5-(2-Hydroxy-phenyl)-3-(2-oxo-2-phenothiazin-10-yl-ethyl)-2-phenyl-3H-tetrazol-2-ium; chloride
CAS No.:129304-01-4
Molecular Formula:C₂₇H₂₀N₅O₂S*Cl
Molecular Weight:514.007
Hs Code.:

Synonyms:5-(2-Hydroxy-phenyl)-3-(2-oxo-2-phenothiazin-10-yl-ethyl)-2-phenyl-3H-tetrazol-2-ium; chloride

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Chemical Property of 5-(2-Hydroxy-phenyl)-3-(2-oxo-2-phenothiazin-10-yl-ethyl)-2-phenyl-3H-tetrazol-2-ium; chloride

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Technology Process of 5-(2-Hydroxy-phenyl)-3-(2-oxo-2-phenothiazin-10-yl-ethyl)-2-phenyl-3H-tetrazol-2-ium; chloride

There total 4 articles about 5-(2-Hydroxy-phenyl)-3-(2-oxo-2-phenothiazin-10-yl-ethyl)-2-phenyl-3H-tetrazol-2-ium; chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 129303-89-5
C₂₇H₂₁N₅O₂S

: 129304-01-4
5-(2-Hydroxy-phenyl)-3-(2-oxo-2-phenothiazin-10-yl-ethyl)-2-phenyl-3H-tetrazol-2-ium; chloride

Guidance literature:: With sulfuric acid; dihydrogen peroxide; iron(II) sulfate; In ethanol; at 100 ℃; for 3h;

Reference yield:

: 54012-74-7
10-(hydrazinoacetyl)-10H-phenothiazine

: 129304-01-4
5-(2-Hydroxy-phenyl)-3-(2-oxo-2-phenothiazin-10-yl-ethyl)-2-phenyl-3H-tetrazol-2-ium; chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / acetic acid / ethanol / 5 h / Heating

2: 1.) sodium nitrite, HCl, glacial acetic acid, 2.) pyridine / 1.) H₂O, 0-5 deg C, 2.) RT, overnight

3: 55 percent / 2N H₂SO₄, FeSO₄, 20percent aq. H₂O₂ / ethanol / 3 h / 100 °C

With pyridine; hydrogenchloride; sulfuric acid; dihydrogen peroxide; iron(II) sulfate; acetic acid; sodium nitrite; In ethanol;

Reference yield:

: 54012-80-5
10-<α-(2-hydroxybenzylidenehydrazino)acetyl>-10H-phenothiazine

: 129304-01-4
5-(2-Hydroxy-phenyl)-3-(2-oxo-2-phenothiazin-10-yl-ethyl)-2-phenyl-3H-tetrazol-2-ium; chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium nitrite, HCl, glacial acetic acid, 2.) pyridine / 1.) H₂O, 0-5 deg C, 2.) RT, overnight

2: 55 percent / 2N H₂SO₄, FeSO₄, 20percent aq. H₂O₂ / ethanol / 3 h / 100 °C

With pyridine; hydrogenchloride; sulfuric acid; dihydrogen peroxide; iron(II) sulfate; acetic acid; sodium nitrite; In ethanol;