N-benzyloxycarbonyl-N-(3,4-dimethoxyphenyl)methyl-2-(phenylthio)ethylamine

Base Information

Chemical Name:N-benzyloxycarbonyl-N-(3,4-dimethoxyphenyl)methyl-2-(phenylthio)ethylamine
CAS No.:191545-69-4
Molecular Formula:C₂₅H₂₇NO₄S
Molecular Weight:437.56
Hs Code.:

Synonyms:N-benzyloxycarbonyl-N-(3,4-dimethoxyphenyl)methyl-2-(phenylthio)ethylamine

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Chemical Property of N-benzyloxycarbonyl-N-(3,4-dimethoxyphenyl)methyl-2-(phenylthio)ethylamine

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Technology Process of N-benzyloxycarbonyl-N-(3,4-dimethoxyphenyl)methyl-2-(phenylthio)ethylamine

There total 3 articles about N-benzyloxycarbonyl-N-(3,4-dimethoxyphenyl)methyl-2-(phenylthio)ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 148679-35-0
N-(3,4-dimethoxyphenyl)methyl-2-(phenylthio)ethylamine

: 191545-69-4
N-benzyloxycarbonyl-N-(3,4-dimethoxyphenyl)methyl-2-(phenylthio)ethylamine

Guidance literature:: With triethylamine; In benzene; for 2h; Ambient temperature;
DOI:10.1248/cpb.45.813

Reference yield:

: 2014-75-7
2-(phenylthio)ethanamine

: 191545-69-4
N-benzyloxycarbonyl-N-(3,4-dimethoxyphenyl)methyl-2-(phenylthio)ethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: AcOH / ethanol / 20 h / Heating

2: NaBH₄ / methanol / 1 h / Ambient temperature

3: 89 percent / Et₃N / benzene / 2 h / Ambient temperature

With sodium tetrahydroborate; acetic acid; triethylamine; In methanol; ethanol; benzene;
DOI:10.1248/cpb.45.813

Reference yield:

: [1-(3,4-Dimethoxy-phenyl)-meth-(Z)-ylidene]-(2-phenylsulfanyl-ethyl)-amine

: 191545-69-4
N-benzyloxycarbonyl-N-(3,4-dimethoxyphenyl)methyl-2-(phenylthio)ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol / 1 h / Ambient temperature

2: 89 percent / Et₃N / benzene / 2 h / Ambient temperature

With sodium tetrahydroborate; triethylamine; In methanol; benzene;
DOI:10.1248/cpb.45.813