C₂₃H₂₈O₂Si

Base Information

Chemical Name:C₂₃H₂₈O₂Si
CAS No.:1447966-32-6
Molecular Formula:C₂₃H₂₈O₂Si
Molecular Weight:364.56
Hs Code.:

C<sub>23</sub>H<sub>28</sub>O<sub>2</sub>Si

Synonyms:C₂₃H₂₈O₂Si

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Chemical Property of C₂₃H₂₈O₂Si

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Technology Process of C₂₃H₂₈O₂Si

There total 4 articles about C₂₃H₂₈O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1447966-24-6
C₃₈H₃₈AuO₂PSi

: 106-95-6
allyl bromide

: 1447966-32-6
C₂₃H₂₈O₂Si

Guidance literature:: With dichloro(1,5-cyclooctadiene)palladium(II); In benzene-d6; at 60 ℃; for 2h; Inert atmosphere; Sealed tube; Schlenk technique;
DOI:10.1002/anie.201303450

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1447966-32-6
C₂₃H₂₈O₂Si

Guidance literature:: Multi-step reaction with 4 steps

1: lithium / tetrahydrofuran / 20 °C / Inert atmosphere; Schlenk technique

2: carbon dioxide / tetrahydrofuran / 0.05 h / 0 °C / Inert atmosphere; Schlenk technique

3: toluene / 8 h / 60 °C / Inert atmosphere; Schlenk technique

4: dichloro(1,5-cyclooctadiene)palladium(II) / benzene-d6 / 2 h / 60 °C / Inert atmosphere; Sealed tube; Schlenk technique

With dichloro(1,5-cyclooctadiene)palladium(II); carbon dioxide; lithium; In tetrahydrofuran; benzene-d6; toluene;
DOI:10.1002/anie.201303450

Reference yield:

: tert-butyldiphenylsilyl lithium

: 1447966-32-6
C₂₃H₂₈O₂Si

Guidance literature:: Multi-step reaction with 3 steps

1: carbon dioxide / tetrahydrofuran / 0.05 h / 0 °C / Inert atmosphere; Schlenk technique

2: toluene / 8 h / 60 °C / Inert atmosphere; Schlenk technique

3: dichloro(1,5-cyclooctadiene)palladium(II) / benzene-d6 / 2 h / 60 °C / Inert atmosphere; Sealed tube; Schlenk technique

With dichloro(1,5-cyclooctadiene)palladium(II); carbon dioxide; In tetrahydrofuran; benzene-d6; toluene;
DOI:10.1002/anie.201303450