Technology Process of 1-chloroheptyl phenyl sulfoxide
There total 1 articles about 1-chloroheptyl phenyl sulfoxide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium diisopropyl amide;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
at -78 ℃;
DOI:10.1016/S0040-4039(01)86017-2
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1) lithium diisopropylamide / 1) THF, -70 deg C, 20 min, 2) THF, -70 deg C, 10 min
2: 93 percent / 30percent aq. KOH / methanol / 1 h / Ambient temperature
3: 89 percent / sodium benzeneselenolate / ethanol / 0.08 h / Ambient temperature
With
potassium hydroxide; sodium phenylselenide; lithium diisopropyl amide;
In
methanol; ethanol;
DOI:10.1246/bcsj.58.1983
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1) lithium diisopropylamide / 1) THF, -70 deg C, 20 min, 2) THF, -70 deg C, 10 min
2: 92 percent / 30percent aq. KOH / methanol / 1 h / Ambient temperature
3: 80 percent / sodium benzeneselenolate / ethanol / 0.08 h / Ambient temperature
With
potassium hydroxide; sodium phenylselenide; lithium diisopropyl amide;
In
methanol; ethanol;
DOI:10.1246/bcsj.58.1983
