1,9-bis(4-tert-butylbenzoyl)-5-mesityldipyrromethane

Base Information

Chemical Name:1,9-bis(4-tert-butylbenzoyl)-5-mesityldipyrromethane
CAS No.:307930-68-3
Molecular Formula:C₄₀H₄₄N₂O₂
Molecular Weight:584.802
Hs Code.:

Synonyms:1,9-bis(4-tert-butylbenzoyl)-5-mesityldipyrromethane

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Chemical Property of 1,9-bis(4-tert-butylbenzoyl)-5-mesityldipyrromethane

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Technology Process of 1,9-bis(4-tert-butylbenzoyl)-5-mesityldipyrromethane

There total 1 articles about 1,9-bis(4-tert-butylbenzoyl)-5-mesityldipyrromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 159152-14-4
5-(mesityl)dipyrromethane

: 1710-98-1
p-tert-butyl benzoyl chloride

: 307930-68-3
1,9-bis(4-tert-butylbenzoyl)-5-mesityldipyrromethane

Guidance literature:: 5-(mesityl)dipyrromethane; With ethylmagnesium bromide; In toluene; at 20 ℃; for 0.5h;

p-tert-butyl benzoyl chloride; In toluene; at 20 ℃; for 0.166667h; Further stages.;
DOI:10.1021/jo000882k

Reference yield: 10.0%

: 863413-54-1
1,1'-bis[bis-(2,2'-pyrryl)methyl]ferrocene

: 307930-68-3
1,9-bis(4-tert-butylbenzoyl)-5-mesityldipyrromethane

: 1,1'-bis[5,10-bis(4-tert-butylphenyl)-15-mesitylporphyrin-20-yl]ferrocene

Guidance literature:: With sodium tetrahydroborate; triethylamine; trifluoroacetic acid; In acetonitrile; NaBH4 added to dipyrromethane in THF-MeOH; stirred (1 h); poured into aq. NH4Cl-CH2Cl2; org. phase washed (H2O), dried (Na2SO4); solvent removed; Fe complex added; dissolved in MeCN; CF3CO2H added; 25 min; DDQ added;stirred (room temp.,1 h); Et3N added; evapd. to dryness; crystd. from THF-CH2Cl2-Et2O-hexane; residue crystd. from THF-ethyl acetate-hexane; elem. anal.;
DOI:10.1039/b505366h