4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-oxobutyramide

Base Information

Chemical Name:4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-oxobutyramide
CAS No.:478162-93-5
Molecular Formula:C₁₉H₂₁NO₃
Molecular Weight:311.381
Hs Code.:

Synonyms:4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-oxobutyramide

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Chemical Property of 4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-oxobutyramide

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Technology Process of 4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-oxobutyramide

There total 7 articles about 4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-oxobutyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 478162-78-6
4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-oxobutyric acid

: 478162-93-5
4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-oxobutyramide

Guidance literature:: With ammonia; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at -40 ℃; for 16h;

Reference yield:

: 478162-80-0
ethyl 4-(3-(2,6-dimethylbenzyloxyl)phenyl)-4-oxobutyrate

: 478162-93-5
4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-oxobutyramide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / ethanol / 3 h / 20 °C

2: triethylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; ammonia / N,N-dimethyl-formamide / 16 h / -40 °C

With ammonia; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; sodium hydroxide; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 187532-78-1
4-(2,6-difluorobenzyloxy)acetophenone

: 478162-93-5
4-(3-(2,6-dimethylbenzyloxy)phenyl)-4-oxobutyramide

Guidance literature:: Multi-step reaction with 4 steps

1: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium hexamethyldisilazane / tetrahydrofuran; ethyl acetate

3: sodium hydroxide; abs ethanol

4: ammonia; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; ammonia; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; sodium hydroxide; abs ethanol; ethyl acetate; N,N-dimethyl-formamide;