O-(2.6-diiodo-4-nitro-phenyl)-N-benzoyl-L-tyrosine ethyl ester

Base Information

• Chemical Name: O-(2.6-diiodo-4-nitro-phenyl)-N-benzoyl-L-tyrosine ethyl ester
• CAS No.: 904808-96-4
• Molecular Formula: C₂₄H₂₀I₂N₂O₆
• Molecular Weight: 686.242
• Mol file: 904808-96-4.mol

Synonyms:O-(2.6-diiodo-4-nitro-phenyl)-N-benzoyl-L-tyrosine ethyl ester

Chemical Property of O-(2.6-diiodo-4-nitro-phenyl)-N-benzoyl-L-tyrosine ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O-(2.6-diiodo-4-nitro-phenyl)-N-benzoyl-L-tyrosine ethyl ester

There total 2 articles about O-(2.6-diiodo-4-nitro-phenyl)-N-benzoyl-L-tyrosine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

L-tyrosine ethyl ester (949-67-7) → O-(2.6-diiodo-4-nitro-phenyl)-N-benzoyl-L-tyrosine ethyl ester (904808-96-4)

Guidance literature:

Multi-step reaction with 2 steps

1: chloroform; aqueous sodium carbonate

2: potassium carbonate; butanone

With chloroform; sodium carbonate; potassium carbonate; butanone;

Reference yield:

N-benzoyl-L-tyrosine ethyl ester (3483-82-7) + 1,2,3-triiodo-5-nitrobenzene (53663-23-3) → O-(2.6-diiodo-4-nitro-phenyl)-N-benzoyl-L-tyrosine ethyl ester (904808-96-4)

Guidance literature:

With potassium carbonate; butanone;

Reference yield:

O-(2.6-diiodo-4-nitro-phenyl)-N-benzoyl-L-tyrosine ethyl ester (904808-96-4) → O-(4-hydroxyphenyl)-3,5-diiodo-L-tyrosine (1596-67-4)

Guidance literature:

Multi-step reaction with 4 steps

1: aq.-ethanolic NaOH-solution

2: aq. NaOH solution / anschliessendes Erwaermen mit Eisen(II)-sulfat und Bariumhydroxid

3: palladium; aq.-ethanolic NaOH-solution / Hydrogenation

4: aqueous hydrochloric acid; sodium nitrite / Erhitzen der Reaktionsloesung mit wss. Salzsaeure

With hydrogenchloride; sodium hydroxide; palladium; sodium nitrite;

upstream raw materials:

N-benzoyl-L-tyrosine ethyl ester

1,2,3-triiodo-5-nitrobenzene

L-tyrosine ethyl ester

Downstream raw materials:

O-(2.6-diiodo-4-nitro-phenyl)-N-benzoyl-L-tyrosine

O-(4-hydroxyphenyl)-3,5-diiodo-L-tyrosine

O-(4-amino-phenyl)-N-benzoyl-L-tyrosine

O-(2.6-diiodo-4-amino-phenyl)-N-benzoyl-L-tyrosine