1-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-1,2,6,7-tetraaza-as-indacen-3-ylamine

Base Information

• Chemical Name: 1-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-1,2,6,7-tetraaza-as-indacen-3-ylamine
• CAS No.: 849663-48-5
• Molecular Formula: C₁₅H₁₅N₅O
• Molecular Weight: 281.317

Synonyms:1-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-1,2,6,7-tetraaza-as-indacen-3-ylamine

Chemical Property of 1-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-1,2,6,7-tetraaza-as-indacen-3-ylamine

Chemical Property:

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Technology Process of 1-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-1,2,6,7-tetraaza-as-indacen-3-ylamine

There total 2 articles about 1-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-1,2,6,7-tetraaza-as-indacen-3-ylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

1-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-1,2,6,7-tetraaza-as-indacene-3-carboxylic acid amide (586353-52-8) → 1-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-1,2,6,7-tetraaza-as-indacen-3-ylamine (849663-48-5)

Guidance literature:

With sodium hydroxide; sodium hypochlorite; at 100 ℃; for 0.25h;

DOI:10.1016/j.bmcl.2005.01.023

Reference yield:

1-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-1,2,6,7-tetraaza-as-indacene-3-carboxylic acid ethyl ester (586353-03-9) → 1-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-1,2,6,7-tetraaza-as-indacen-3-ylamine (849663-48-5)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. NH₃ / methanol / 25 - 60 °C

2: 76 percent / NaOH; NaClO / 0.25 h / 100 °C

With ammonium hydroxide; sodium hydroxide; sodium hypochlorite; In methanol;

DOI:10.1016/j.bmcl.2005.01.023

Reference yield:

1-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-1,2,6,7-tetraaza-as-indacen-3-ylamine (849663-48-5) → 1-(4-methoxy-phenyl)-1,6-dihydro-1,2,6,7-tetraaza-as-indacen-3-ylamine

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; at 100 ℃; for 2.5h;

DOI:10.1016/j.bmcl.2005.01.023

upstream raw materials:

1-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-1,2,6,7-tetraaza-as-indacene-3-carboxylic acid amide

1-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-1,2,6,7-tetraaza-as-indacene-3-carboxylic acid ethyl ester

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