C₂₃H₂₆N₄O₂

Base Information

Chemical Name:C₂₃H₂₆N₄O₂
CAS No.:1049633-06-8
Molecular Formula:C₂₃H₂₆N₄O₂
Molecular Weight:390.485
Hs Code.:

C<sub>23</sub>H<sub>26</sub>N<sub>4</sub>O<sub>2</sub>

Synonyms:C₂₃H₂₆N₄O₂

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Chemical Property of C₂₃H₂₆N₄O₂

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Technology Process of C₂₃H₂₆N₄O₂

There total 7 articles about C₂₃H₂₆N₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1049634-33-4
C₂₈H₃₄N₄O₄

: 1049633-06-8
C₂₃H₂₆N₄O₂

Guidance literature:: C₂₈H₃₄N₄O₄; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1.5h;

With ammonia; In methanol; dichloromethane;

Reference yield:

: 1049633-96-6
C₁₀H₉NO₄

: 1049633-06-8
C₂₃H₂₆N₄O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: ethylmagnesium bromide / diethyl ether; dichloromethane / 1 h / -20 °C

1.2: 0.5 h / -20 - 20 °C

2.1: methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 - 20 °C

2.2: 1.5 h / 65 °C

2.3: 20 °C

3.1: hydrogen / 10 % Pd(OH)2/C / methanol / 12 h / 2068.65 Torr

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C

5.1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C

With ethylmagnesium bromide; hydrogen; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; 10 % Pd(OH)2/C; In methanol; diethyl ether; dichloromethane;

Reference yield:

: 1049633-95-5
C₁₁H₁₁NO₄

: 1049633-06-8
C₂₃H₂₆N₄O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: formic acid / 2 h / 90 °C

2.1: ethylmagnesium bromide / diethyl ether; dichloromethane / 1 h / -20 °C

2.2: 0.5 h / -20 - 20 °C

3.1: methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 - 20 °C

3.2: 1.5 h / 65 °C

3.3: 20 °C

4.1: hydrogen / 10 % Pd(OH)2/C / methanol / 12 h / 2068.65 Torr

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C

6.1: trifluoroacetic acid / dichloromethane / 1.5 h / 20 °C

With formic acid; ethylmagnesium bromide; hydrogen; methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; 10 % Pd(OH)2/C; In methanol; diethyl ether; dichloromethane;