1-[(perfluorooctylpropysulfonylethyl)-(2-cyanoethyl)-phosphate]-2-O-benzyl-sn-glycerol

Base Information

Chemical Name:1-[(perfluorooctylpropysulfonylethyl)-(2-cyanoethyl)-phosphate]-2-O-benzyl-sn-glycerol
CAS No.:1354914-06-9
Molecular Formula:C₂₆H₂₇F₁₇NO₈PS
Molecular Weight:867.515
Hs Code.:

Synonyms:1-[(perfluorooctylpropysulfonylethyl)-(2-cyanoethyl)-phosphate]-2-O-benzyl-sn-glycerol

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Chemical Property of 1-[(perfluorooctylpropysulfonylethyl)-(2-cyanoethyl)-phosphate]-2-O-benzyl-sn-glycerol

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Technology Process of 1-[(perfluorooctylpropysulfonylethyl)-(2-cyanoethyl)-phosphate]-2-O-benzyl-sn-glycerol

There total 4 articles about 1-[(perfluorooctylpropysulfonylethyl)-(2-cyanoethyl)-phosphate]-2-O-benzyl-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₇H₄₅F₁₇NO₁₀PS

: 1354914-06-9
1-[(perfluorooctylpropysulfonylethyl)-(2-cyanoethyl)-phosphate]-2-O-benzyl-sn-glycerol

Guidance literature:: With triethylsilane; dichloro-acetic acid; In dichloromethane; toluene; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol2033652

Reference yield:

: 1154463-63-4
2-[3-(perfluorooctyl)propylsulfonyl]ethanol

: 1354914-06-9
1-[(perfluorooctylpropysulfonylethyl)-(2-cyanoethyl)-phosphate]-2-O-benzyl-sn-glycerol

Guidance literature:: Multi-step reaction with 3 steps

1: 4,5-dicyano-1H-imidazole / acetonitrile / 1 h / 20 °C / Inert atmosphere; Molecular sieve

2: pyridine; water; iodine / tetrahydrofuran / 0.08 h / 20 °C / Inert atmosphere

3: triethylsilane; dichloro-acetic acid / dichloromethane; toluene / 0.5 h / 20 °C / Inert atmosphere

With pyridine; triethylsilane; dichloro-acetic acid; 4,5-dicyano-1H-imidazole; water; iodine; In tetrahydrofuran; dichloromethane; toluene; acetonitrile;
DOI:10.1021/ol2033652

Reference yield:

: 1235579-72-2
1-([N,N-diisopropylamino]-2-cyanoethylphosphite)-2-O-benzyl-3-O-(4,4'-dimethoxytrityl)-sn-glycerol

: 1354914-06-9
1-[(perfluorooctylpropysulfonylethyl)-(2-cyanoethyl)-phosphate]-2-O-benzyl-sn-glycerol

Guidance literature:: Multi-step reaction with 3 steps

1: 4,5-dicyano-1H-imidazole / acetonitrile / 1 h / 20 °C / Inert atmosphere; Molecular sieve

2: pyridine; water; iodine / tetrahydrofuran / 0.08 h / 20 °C / Inert atmosphere

3: triethylsilane; dichloro-acetic acid / dichloromethane; toluene / 0.5 h / 20 °C / Inert atmosphere

With pyridine; triethylsilane; dichloro-acetic acid; 4,5-dicyano-1H-imidazole; water; iodine; In tetrahydrofuran; dichloromethane; toluene; acetonitrile;
DOI:10.1021/ol2033652