N-tent-butyl-7-methoxy-N-methyl-8-(2-(4-methylpiperazin-1-yl)acetamido)-1-m-tolyl-4,5-dihydro-1H-benzo[g]indazole-3-carboxamide

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Chemical Name:N-tent-butyl-7-methoxy-N-methyl-8-(2-(4-methylpiperazin-1-yl)acetamido)-1-m-tolyl-4,5-dihydro-1H-benzo[g]indazole-3-carboxamide
CAS No.:1262800-29-2
Molecular Formula:C₃₂H₄₂N₆O₃
Molecular Weight:558.724
Hs Code.:

Synonyms:N-tent-butyl-7-methoxy-N-methyl-8-(2-(4-methylpiperazin-1-yl)acetamido)-1-m-tolyl-4,5-dihydro-1H-benzo[g]indazole-3-carboxamide

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Chemical Property of N-tent-butyl-7-methoxy-N-methyl-8-(2-(4-methylpiperazin-1-yl)acetamido)-1-m-tolyl-4,5-dihydro-1H-benzo[g]indazole-3-carboxamide

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Technology Process of N-tent-butyl-7-methoxy-N-methyl-8-(2-(4-methylpiperazin-1-yl)acetamido)-1-m-tolyl-4,5-dihydro-1H-benzo[g]indazole-3-carboxamide

There total 3 articles about N-tent-butyl-7-methoxy-N-methyl-8-(2-(4-methylpiperazin-1-yl)acetamido)-1-m-tolyl-4,5-dihydro-1H-benzo[g]indazole-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-01-3
1-methyl-piperazine

: 1262800-38-3
C₂₇H₃₁BrN₄O₃

: 1262800-29-2
N-tent-butyl-7-methoxy-N-methyl-8-(2-(4-methylpiperazin-1-yl)acetamido)-1-m-tolyl-4,5-dihydro-1H-benzo[g]indazole-3-carboxamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 16h;

Reference yield:

: 1262800-33-8
C₂₅H₂₈BrN₃O₂

: 1262800-29-2
N-tent-butyl-7-methoxy-N-methyl-8-(2-(4-methylpiperazin-1-yl)acetamido)-1-m-tolyl-4,5-dihydro-1H-benzo[g]indazole-3-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hexamethyldisilazane; CyJohnPhos; 1,1,1-triphenylsilylamine / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; tetrahydrofuran / 4 h / 100 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C

With 1,1,1-triphenylsilylamine; N-ethyl-N,N-diisopropylamine; lithium hexamethyldisilazane; CyJohnPhos; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 1262800-35-0
C₂₅H₃₀N₄O₂

: 1262800-29-2
N-tent-butyl-7-methoxy-N-methyl-8-(2-(4-methylpiperazin-1-yl)acetamido)-1-m-tolyl-4,5-dihydro-1H-benzo[g]indazole-3-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C

With N-ethyl-N,N-diisopropylamine; In dichloromethane;