C₂₀H₂₀BNO₆

Base Information

• Chemical Name: C₂₀H₂₀BNO₆
• CAS No.: 1362479-66-0
• Molecular Formula: C₂₀H₂₀BNO₆
• Molecular Weight: 381.193

Synonyms:C₂₀H₂₀BNO₆

Chemical Property of C₂₀H₂₀BNO₆

Chemical Property:

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Technology Process of C₂₀H₂₀BNO₆

There total 1 articles about C₂₀H₂₀BNO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

indomethacin methyl ester (1601-18-9) → C20H20BNO6 (1362479-66-0) + C60H54B3N3O15

Guidance literature:

indomethacin methyl ester; With tetrahydroxydiboron; chloro(2-dicyclohexylphosphino-2’,4’,6’-triisopropyl-1,1‘-biphenyl)[2-(2’-amino-1,1‘-biphenyl’)]palladium(II); potassium acetate; sodium t-butanolate; XPhos; In ethanol; at 80 ℃; for 3h; Inert atmosphere;

With hydrogenchloride; In ethanol; water; ethyl acetate; for 0.5h;

DOI:10.1021/ol300364s

Reference yield: 86.0%

C20H20BNO6 (1362479-66-0) → C20H18INO4

Guidance literature:

With iodine; potassium carbonate; In acetonitrile; at 80 ℃; for 12h; Inert atmosphere; Schlenk technique; Sealed tube;

DOI:10.1002/anie.201803228

Reference yield: 45.0%

C20H20BNO6 (1362479-66-0) + N-ethynyl-4-methyl-N-2-propan-1-yl-benzenesulfonamide (312329-85-4) → methyl 2-(5-methoxy-2-methyl-1-(4-((5-oxo-1-tosylpyrrolidin-3-yl)methyl)benzoyl)-1H-indol-3-yl)acetate

Guidance literature:

N-ethynyl-4-methyl-N-2-propan-1-yl-benzenesulfonamide; With N-hydroxyphthalimide; In dichloromethane; for 6h; Inert atmosphere; Reflux;

C₂₀H₂₀BNO₆; With triethylamine; In 1,4-dioxane; at 85 ℃; for 3h;

DOI:10.1039/c7cc07055a

upstream raw materials:

indomethacin methyl ester

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