(S)-3-(4-chlorophenyl)-2-((2R,3S,4R)-3,4-dihydroxy pyrrolidin-2-yl)thiazolidin-4-one

Base Information

Chemical Name:(S)-3-(4-chlorophenyl)-2-((2R,3S,4R)-3,4-dihydroxy pyrrolidin-2-yl)thiazolidin-4-one
CAS No.:1430376-09-2
Molecular Formula:C₁₃H₁₅ClN₂O₃S
Molecular Weight:314.793
Hs Code.:

Synonyms:(S)-3-(4-chlorophenyl)-2-((2R,3S,4R)-3,4-dihydroxy pyrrolidin-2-yl)thiazolidin-4-one

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Chemical Property of (S)-3-(4-chlorophenyl)-2-((2R,3S,4R)-3,4-dihydroxy pyrrolidin-2-yl)thiazolidin-4-one

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Technology Process of (S)-3-(4-chlorophenyl)-2-((2R,3S,4R)-3,4-dihydroxy pyrrolidin-2-yl)thiazolidin-4-one

There total 2 articles about (S)-3-(4-chlorophenyl)-2-((2R,3S,4R)-3,4-dihydroxy pyrrolidin-2-yl)thiazolidin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1430375-94-2
(3aS,4R,6aR)-tert-butyl 4-((S)-3-(4-chlorophenyl)-4-oxothiazolidin-2-yl)-2,2-dimethyldihydro-3aH-[1,3]dioxolo[4,5-c]pyrrole-5(4H)-carboxylate

: 1430376-09-2
(S)-3-(4-chlorophenyl)-2-((2R,3S,4R)-3,4-dihydroxy pyrrolidin-2-yl)thiazolidin-4-one

Guidance literature:: With trifluoroacetic acid; In water; at 20 ℃; for 1h;
DOI:10.1016/j.tetasy.2013.03.006

Reference yield:

: 1189331-75-6
tert-butyl (3aS,4R,6aR)-2,2-dimethyl-4-formyldihydro-3aH-[1,3]dioxolane[4,5-c]pyrrol-5-(4H)-carboxylate

: 1430376-09-2
(S)-3-(4-chlorophenyl)-2-((2R,3S,4R)-3,4-dihydroxy pyrrolidin-2-yl)thiazolidin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / 1 h / 40 °C / Inert atmosphere

1.2: 12 h / 40 °C / Inert atmosphere

2.1: trifluoroacetic acid / water / 1 h / 20 °C

With trifluoroacetic acid; In water; toluene;
DOI:10.1016/j.tetasy.2013.03.006