C₂₂H₂₃⁽³⁾HN₂O₂

Base Information

Chemical Name:C₂₂H₂₃⁽³⁾HN₂O₂
CAS No.:133008-50-1
Molecular Formula:C₂₂H₂₄N₂O₂
Molecular Weight:350.437
Hs Code.:

C<sub>22</sub>H<sub>23</sub><sup>(3)</sup>HN<sub>2</sub>O<sub>2</sub>

Synonyms:C₂₂H₂₃⁽³⁾HN₂O₂

Suppliers and Price of C₂₂H₂₃⁽³⁾HN₂O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₃⁽³⁾HN₂O₂

Chemical Property:

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Technology Process of C₂₂H₂₃⁽³⁾HN₂O₂

There total 11 articles about C₂₂H₂₃⁽³⁾HN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 133008-49-8
C₂₂H₂₁⁽³⁾HN₄O₂

: 133008-50-1
C₂₂H₂₃⁽³⁾HN₂O₂

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran;

Reference yield:

: 26866-40-0
3,5'-O-dibenzylpyridoxal

: 133008-50-1
C₂₂H₂₃⁽³⁾HN₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / NaBT₄ / tetrahydrofuran

2: 94 percent / pyridinium chlorochromate, NaOAc / CH₂Cl₂

3: (R)-alpine-borane / tetrahydrofuran

4: DEAD, ZnN₆*2Pyr, Ph₃P / toluene

5: LiAlH₄ / tetrahydrofuran

With lithium aluminium tetrahydride; sodium boron [ 3H]hydride; B-isopinocampheyl-9-borabicyclo[3.3.1]nonane; ZnN₆*2Pyr; sodium acetate; triphenylphosphine; pyridinium chlorochromate; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 65-23-6
5-hydroxy-6-methyl-3,4-pyridinedimethanol

: 133008-50-1
C₂₂H₂₃⁽³⁾HN₂O₂

Guidance literature:: Multi-step reaction with 9 steps

1: 1.) TsOH, 2.) NaH / 1.) acetone, 2.) THF

2: HCOOH

3: NaOMe / methanol

4: pyridinium chlorochromate, NaOAc / CH₂Cl₂

5: 85 percent / NaBT₄ / tetrahydrofuran

6: 94 percent / pyridinium chlorochromate, NaOAc / CH₂Cl₂

7: (R)-alpine-borane / tetrahydrofuran

8: DEAD, ZnN₆*2Pyr, Ph₃P / toluene

9: LiAlH₄ / tetrahydrofuran

With lithium aluminium tetrahydride; formic acid; sodium boron [ 3H]hydride; B-isopinocampheyl-9-borabicyclo[3.3.1]nonane; ZnN₆*2Pyr; sodium methylate; sodium acetate; sodium hydride; toluene-4-sulfonic acid; triphenylphosphine; pyridinium chlorochromate; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; toluene;