(2R,3S)-2-tert-butoxycarbonylamino-4-(p-methoxybenzyloxy)-3-methylbutanal

Base Information

Chemical Name:(2R,3S)-2-tert-butoxycarbonylamino-4-(p-methoxybenzyloxy)-3-methylbutanal
CAS No.:238746-09-3
Molecular Formula:C₁₈H₂₇NO₅
Molecular Weight:337.416
Hs Code.:

Synonyms:(2R,3S)-2-tert-butoxycarbonylamino-4-(p-methoxybenzyloxy)-3-methylbutanal

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Chemical Property of (2R,3S)-2-tert-butoxycarbonylamino-4-(p-methoxybenzyloxy)-3-methylbutanal

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Technology Process of (2R,3S)-2-tert-butoxycarbonylamino-4-(p-methoxybenzyloxy)-3-methylbutanal

There total 5 articles about (2R,3S)-2-tert-butoxycarbonylamino-4-(p-methoxybenzyloxy)-3-methylbutanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 238746-07-1
(2R,3S)-2-tert-butoxycarbonylamino-4-(p-methoxybenzyloxy)-3-methylbutanal

: 238746-09-3
(2R,3S)-2-tert-butoxycarbonylamino-4-(p-methoxybenzyloxy)-3-methylbutanal

Guidance literature:: With Dess-Martin periodane; In dichloromethane; for 1h;
DOI:10.1021/ja9811243

Reference yield:

: 238746-03-7
(2R,3S)-2-azido-4-(p-methoxybenzyloxy)-3-methyl-1-butanol

: 238746-09-3
(2R,3S)-2-tert-butoxycarbonylamino-4-(p-methoxybenzyloxy)-3-methylbutanal

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / H₂ / 10 percent Pd/C / methanol / 0.67 h

2: CH₂Cl₂

3: 94 percent / Dess-Martin reagent / CH₂Cl₂ / 1 h

With hydrogen; Dess-Martin periodane; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/ja9811243

Reference yield:

: (1R,2R,6S,8R)-4-[(2S,3S)-2-Azido-4-(4-methoxy-benzyloxy)-3-methyl-butyl]-2,9,9-trimethyl-3,5-dioxa-4-bora-tricyclo[6.1.1.0^2,6]decane

: 238746-09-3
(2R,3S)-2-tert-butoxycarbonylamino-4-(p-methoxybenzyloxy)-3-methylbutanal

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / H₂O₂, aq. NaOH

2: 100 percent / H₂ / 10 percent Pd/C / methanol / 0.67 h

3: CH₂Cl₂

4: 94 percent / Dess-Martin reagent / CH₂Cl₂ / 1 h

With sodium hydroxide; hydrogen; dihydrogen peroxide; Dess-Martin periodane; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/ja9811243