2-C-(3,4,6-tri-O-benzyl)-galactal aldoxime

Base Information

• Chemical Name: 2-C-(3,4,6-tri-O-benzyl)-galactal aldoxime
• CAS No.: 1064077-76-4
• Molecular Formula: C₂₈H₂₉NO₅
• Molecular Weight: 459.542

Synonyms:2-C-(3,4,6-tri-O-benzyl)-galactal aldoxime

Chemical Property of 2-C-(3,4,6-tri-O-benzyl)-galactal aldoxime

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Technology Process of 2-C-(3,4,6-tri-O-benzyl)-galactal aldoxime

There total 1 articles about 2-C-(3,4,6-tri-O-benzyl)-galactal aldoxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

(2R,3R,4R)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-3,4-dihydro-2H-pyran-5-carbaldehyde (136982-88-2) → 2-C-(3,4,6-tri-O-benzyl)-galactal aldoxime (1064077-76-4)

Guidance literature:

With hydroxylamine hydrochloride; sodium acetate; In tetrahydrofuran; water; at 20 ℃; for 15h;

DOI:10.1021/jo801337k

Reference yield: 64.0%

2-C-(3,4,6-tri-O-benzyl)-galactal aldoxime (1064077-76-4) + ethyl cinnamate (4192-77-2) → 3-(2-C-3,4,6-tri-O-benzylgalactal)-5-ethoxycarbonyl-4-phenyl-Δ2-isoxazoline (1064075-27-9)

Guidance literature:

With iodosylbenzene; cetyltrimethylammonim bromide; In water; at 20 ℃; for 3.5h;

DOI:10.1021/jo801337k

Reference yield: 58.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 2-C-(3,4,6-tri-O-benzyl)-galactal aldoxime (1064077-76-4) → 3-(2-C-3,4,6-tri-O-benzylgalactal)-5-phenyl-Δ2-isoxazoline

Guidance literature:

With iodosylbenzene; cetyltrimethylammonim bromide; In water; at 20 ℃; for 3h;

DOI:10.1021/jo801337k

upstream raw materials:

(2R,3R,4R)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-3,4-dihydro-2H-pyran-5-carbaldehyde

Downstream raw materials:

3-(2-C-3,4,6-tri-O-benzylgalactal)-5-ethoxycarbonyl-4-phenyl-Δ²-isoxazoline

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