Technology Process of exo-6-benzyl-1-aminomethylbicyclo<2.2.2>-2-octene
There total 9 articles about exo-6-benzyl-1-aminomethylbicyclo<2.2.2>-2-octene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium;
In
tetrahydrofuran; ammonia;
for 2h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 13 percent / hydroquinone / 24 h / 150 °C
2: sodium ethoxide / ethanol / 72 h / Ambient temperature
3: 87 percent / KOH / ethanol / 4 h / Heating
4: 100 percent / SOCl2 / CHCl3 / 3 h / Heating
5: 61 percent / gaseous NH3 / tetrahydrofuran / 144 h / Ambient temperature
6: 33 percent / LAH / tetrahydrofuran / 24 h / Heating
7: 84 percent / Li / tetrahydrofuran; liquid ammonia / 2 h
With
potassium hydroxide; lithium aluminium tetrahydride; thionyl chloride; ammonia; sodium ethanolate; lithium; hydroquinone;
In
tetrahydrofuran; ethanol; chloroform; ammonia;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 13 percent / hydroquinone / 24 h / 150 °C
2: sodium ethoxide / ethanol / 72 h / Ambient temperature
3: 87 percent / KOH / ethanol / 4 h / Heating
4: 100 percent / SOCl2 / CHCl3 / 3 h / Heating
5: 61 percent / gaseous NH3 / tetrahydrofuran / 144 h / Ambient temperature
6: 33 percent / LAH / tetrahydrofuran / 24 h / Heating
7: 84 percent / Li / tetrahydrofuran; liquid ammonia / 2 h
With
potassium hydroxide; lithium aluminium tetrahydride; thionyl chloride; ammonia; sodium ethanolate; lithium; hydroquinone;
In
tetrahydrofuran; ethanol; chloroform; ammonia;
