Technology Process of 2-<2-(butyl-1,3-dioxolan-2-yl)ethyl>benzenamine
There total 4 articles about 2-<2-(butyl-1,3-dioxolan-2-yl)ethyl>benzenamine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethanol;
DOI:10.1055/s-1994-25615
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 74 percent / tetrahydrofuran; diethyl ether / 1 h / 0 °C
2: 99 percent / tetrabutylammonium chloride, palladium(II) acetate, NaHCO3 / dimethylformamide / 7 h / 50 °C
3: 60 percent / p-toluenesulfonic acid monohydrate / toluene / 18 h / Heating
4: 98 percent / hydrogen / 10percent palladium on carbon / ethanol
With
tetrabutyl-ammonium chloride; hydrogen; palladium diacetate; sodium hydrogencarbonate; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
tetrahydrofuran; diethyl ether; ethanol; N,N-dimethyl-formamide; toluene;
DOI:10.1055/s-1994-25615
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 99 percent / tetrabutylammonium chloride, palladium(II) acetate, NaHCO3 / dimethylformamide / 7 h / 50 °C
2: 60 percent / p-toluenesulfonic acid monohydrate / toluene / 18 h / Heating
3: 98 percent / hydrogen / 10percent palladium on carbon / ethanol
With
tetrabutyl-ammonium chloride; hydrogen; palladium diacetate; sodium hydrogencarbonate; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
ethanol; N,N-dimethyl-formamide; toluene;
DOI:10.1055/s-1994-25615
