1-(2,4-dimethyl-5-thiazolyl)-2-[2-methyl-5-(4-methylphenyl)-3-thienyl]perfluorocyclopentene

Base Information

• Chemical Name: 1-(2,4-dimethyl-5-thiazolyl)-2-[2-methyl-5-(4-methylphenyl)-3-thienyl]perfluorocyclopentene
• CAS No.: 1255910-32-7
• Molecular Formula: C₂₂H₁₇F₆NS₂
• Molecular Weight: 473.506

Synonyms:1-(2,4-dimethyl-5-thiazolyl)-2-[2-methyl-5-(4-methylphenyl)-3-thienyl]perfluorocyclopentene

Chemical Property of 1-(2,4-dimethyl-5-thiazolyl)-2-[2-methyl-5-(4-methylphenyl)-3-thienyl]perfluorocyclopentene

Chemical Property:

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Technology Process of 1-(2,4-dimethyl-5-thiazolyl)-2-[2-methyl-5-(4-methylphenyl)-3-thienyl]perfluorocyclopentene

There total 2 articles about 1-(2,4-dimethyl-5-thiazolyl)-2-[2-methyl-5-(4-methylphenyl)-3-thienyl]perfluorocyclopentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

1-(2,4-dimethyl-5-thiazolyl)perfluorocyclopentene (1201898-68-1) + 3-bromo-2-methyl-5-(4-methylphenyl)thiophene → 1-(2,4-dimethyl-5-thiazolyl)-2-[2-methyl-5-(4-methylphenyl)-3-thienyl]perfluorocyclopentene (1255910-32-7)

Guidance literature:

3-bromo-2-methyl-5-(4-methylphenyl)thiophene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

1-(2,4-dimethyl-5-thiazolyl)perfluorocyclopentene; In tetrahydrofuran; hexane; at -78 ℃; for 2h; Inert atmosphere;

DOI:10.1016/j.tet.2010.09.066

Reference yield:

C22H17F6NS2 (1255910-35-0) → 1-(2,4-dimethyl-5-thiazolyl)-2-[2-methyl-5-(4-methylphenyl)-3-thienyl]perfluorocyclopentene (1255910-32-7)

Guidance literature:

In hexane; at 20 ℃; Solvent; Quantum yield; Visible light irradiation;

DOI:10.1016/j.tet.2010.09.066

Reference yield:

1-(2,4-dimethyl-5-thiazolyl)-2-[2-methyl-5-(4-methylphenyl)-3-thienyl]perfluorocyclopentene (1255910-32-7) → C22H17F6NS2 (1255910-35-0)

Guidance literature:

In hexane; at 20 ℃; Solvent; Quantum yield; UV-irradiation;

DOI:10.1016/j.tet.2010.09.066

upstream raw materials:

1-(2,4-dimethyl-5-thiazolyl)perfluorocyclopentene

C₂₂H₁₇F₆NS₂

Downstream raw materials:

C₂₂H₁₇F₆NS₂

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