(2,4-dichloro-3-phenylquinolin-6-yl)(1-methylpiperidin-3-yl)pyridin-3-ylmethanol trifluoroacetate

Base Information

Chemical Name:(2,4-dichloro-3-phenylquinolin-6-yl)(1-methylpiperidin-3-yl)pyridin-3-ylmethanol trifluoroacetate
CAS No.:1600565-01-2
Molecular Formula:C₂HF₃O₂*C₂₇H₂₅Cl₂N₃O
Molecular Weight:592.445
Hs Code.:

Synonyms:(2,4-dichloro-3-phenylquinolin-6-yl)(1-methylpiperidin-3-yl)pyridin-3-ylmethanol trifluoroacetate

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Chemical Property of (2,4-dichloro-3-phenylquinolin-6-yl)(1-methylpiperidin-3-yl)pyridin-3-ylmethanol trifluoroacetate

Chemical Property:

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Technology Process of (2,4-dichloro-3-phenylquinolin-6-yl)(1-methylpiperidin-3-yl)pyridin-3-ylmethanol trifluoroacetate

There total 9 articles about (2,4-dichloro-3-phenylquinolin-6-yl)(1-methylpiperidin-3-yl)pyridin-3-ylmethanol trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1600564-99-5
(2,4-dichloro-3-phenylquinolin-6-yl)(piperidin-3-yl)pyridin-3-ylmethanol trifluoroacetate

: 1600565-01-2
(2,4-dichloro-3-phenylquinolin-6-yl)(1-methylpiperidin-3-yl)pyridin-3-ylmethanol trifluoroacetate

Guidance literature:: With sodium cyanoborohydride; In methanol; water;

Reference yield:

: 452349-62-1
methyl 5-bromo-2-(2-phenylacetamido)benzoate

: 1600565-01-2
(2,4-dichloro-3-phenylquinolin-6-yl)(1-methylpiperidin-3-yl)pyridin-3-ylmethanol trifluoroacetate

Guidance literature:: Multi-step reaction with 5 steps

1: lithium hexamethyldisilazane / tetrahydrofuran; hexane; water / 4 h / -78 - 20 °C

2: trichlorophosphate / 3.5 h / 107 °C

3: n-butyllithium / tetrahydrofuran; hexane / 3 h / -78 - 0 °C

4: 1 h / 20 °C

5: sodium cyanoborohydride / water; methanol

With n-butyllithium; sodium cyanoborohydride; lithium hexamethyldisilazane; trichlorophosphate; In tetrahydrofuran; methanol; hexane; water;

Reference yield:

: 909365-96-4
6-bromo-4-hydroxy-3-phenylquinolin-2(1H)-one

: 1600565-01-2
(2,4-dichloro-3-phenylquinolin-6-yl)(1-methylpiperidin-3-yl)pyridin-3-ylmethanol trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate / 3.5 h / 107 °C

2: n-butyllithium / tetrahydrofuran; hexane / 3 h / -78 - 0 °C

3: 1 h / 20 °C

4: sodium cyanoborohydride / water; methanol

With n-butyllithium; sodium cyanoborohydride; trichlorophosphate; In tetrahydrofuran; methanol; hexane; water;