phenyl 2,6-di-O-benzoyl-4-O-{2-[(tert-butoxycarbonyl)(1-ethylpropyl)amino]acetyl}-3-O-{2-[(1-ethylpropyl)(9H-fluoren-9-ylmethoxycarbonyl)amino]acetyl}-1-thio-β-D-galactopyranoside

Base Information

• Chemical Name: phenyl 2,6-di-O-benzoyl-4-O-{2-[(tert-butoxycarbonyl)(1-ethylpropyl)amino]acetyl}-3-O-{2-[(1-ethylpropyl)(9H-fluoren-9-ylmethoxycarbonyl)amino]acetyl}-1-thio-β-D-galactopyranoside
• CAS No.: 1054604-97-5
• Molecular Formula: C₆₀H₆₈N₂O₁₃S
• Molecular Weight: 1057.27
• Mol file: 1054604-97-5.mol

Synonyms:phenyl 2,6-di-O-benzoyl-4-O-{2-[(tert-butoxycarbonyl)(1-ethylpropyl)amino]acetyl}-3-O-{2-[(1-ethylpropyl)(9H-fluoren-9-ylmethoxycarbonyl)amino]acetyl}-1-thio-β-D-galactopyranoside

Chemical Property of phenyl 2,6-di-O-benzoyl-4-O-{2-[(tert-butoxycarbonyl)(1-ethylpropyl)amino]acetyl}-3-O-{2-[(1-ethylpropyl)(9H-fluoren-9-ylmethoxycarbonyl)amino]acetyl}-1-thio-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenyl 2,6-di-O-benzoyl-4-O-{2-[(tert-butoxycarbonyl)(1-ethylpropyl)amino]acetyl}-3-O-{2-[(1-ethylpropyl)(9H-fluoren-9-ylmethoxycarbonyl)amino]acetyl}-1-thio-β-D-galactopyranoside

There total 1 articles about phenyl 2,6-di-O-benzoyl-4-O-{2-[(tert-butoxycarbonyl)(1-ethylpropyl)amino]acetyl}-3-O-{2-[(1-ethylpropyl)(9H-fluoren-9-ylmethoxycarbonyl)amino]acetyl}-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-[(tert-butoxycarbonyl)(1-ethylpropyl)amino]acetic acid (1054604-69-1) + phenyl 2,6-di-O-benzoyl-3-O-{2-[(1-ethylpropyl)(9H-fluoren-9-ylmethoxycarbonyl)amino]acetyl}-1-thio-β-D-galactopyranoside (1054604-95-3) → phenyl 2,6-di-O-benzoyl-4-O-{2-[(tert-butoxycarbonyl)(1-ethylpropyl)amino]acetyl}-3-O-{2-[(1-ethylpropyl)(9H-fluoren-9-ylmethoxycarbonyl)amino]acetyl}-1-thio-β-D-galactopyranoside (1054604-97-5)

Guidance literature:

With dmap; diisopropyl-carbodiimide; In dichloromethane; at 0 ℃; for 2h;

DOI:10.1080/07328300903100661

Reference yield:

C10H10NO4Pol + phenyl 2,6-di-O-benzoyl-4-O-{2-[(tert-butoxycarbonyl)(1-ethylpropyl)amino]acetyl}-3-O-{2-[(1-ethylpropyl)(9H-fluoren-9-ylmethoxycarbonyl)amino]acetyl}-1-thio-β-D-galactopyranoside (1054604-97-5) → C10H11NO4 (264618-14-6) + C16H21NO9 (1054605-30-9)

Guidance literature:

C₁₀H₁₀NO₄Pol; phenyl 2,6-di-O-benzoyl-4-O-{2-[(tert-butoxycarbonyl)(1-ethylpropyl)amino]acetyl}-3-O-{2-[(1-ethylpropyl)(9H-fluoren-9-ylmethoxycarbonyl)amino]acetyl}-1-thio-β-D-galactopyranoside; With dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In dichloromethane; at 20 ℃; for 24h; solid phase reaction;

With sodium methylate; In methanol; dichloromethane; at 20 ℃; for 1h; solid phase reaction;

With water; In methanol; dichloromethane; at 20 ℃; for 1h;

DOI:10.1080/07328300903100661

upstream raw materials:

2-[(tert-butoxycarbonyl)(1-ethylpropyl)amino]acetic acid

phenyl 2,6-di-O-benzoyl-3-O-{2-[(1-ethylpropyl)(9H-fluoren-9-ylmethoxycarbonyl)amino]acetyl}-1-thio-β-D-galactopyranoside

Downstream raw materials:

C₁₀H₁₁NO₄

C₁₆H₂₁NO₉