4-nitro-N-((5-oxo-2-phenyltetrahydrofuran-2-yl)methyl)benzenesulfonamide

Base Information

Chemical Name:4-nitro-N-((5-oxo-2-phenyltetrahydrofuran-2-yl)methyl)benzenesulfonamide
CAS No.:1338575-80-6
Molecular Formula:C₁₇H₁₆N₂O₆S
Molecular Weight:376.39
Hs Code.:

Synonyms:4-nitro-N-((5-oxo-2-phenyltetrahydrofuran-2-yl)methyl)benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-nitro-N-((5-oxo-2-phenyltetrahydrofuran-2-yl)methyl)benzenesulfonamide

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Technology Process of 4-nitro-N-((5-oxo-2-phenyltetrahydrofuran-2-yl)methyl)benzenesulfonamide

There total 2 articles about 4-nitro-N-((5-oxo-2-phenyltetrahydrofuran-2-yl)methyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 869811-06-3
4-phenylpent-4-enoic acid tert-butyl ester

: 6325-93-5
p-nitrobenzenesulfonamide

: 1338575-80-6
4-nitro-N-((5-oxo-2-phenyltetrahydrofuran-2-yl)methyl)benzenesulfonamide

Guidance literature:: With tetrakis(actonitrile)copper(I) hexafluorophosphate; iodosylbenzene; ethylenediamine; In acetonitrile; at 20 ℃; for 48h; Molecular sieve;
DOI:10.1021/ol202436a

Reference yield:

: 92975-38-7
4-bromo-4-pentenoic acid tert-butyl ester

: 1338575-80-6
4-nitro-N-((5-oxo-2-phenyltetrahydrofuran-2-yl)methyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: barium hydroxide octahydrate; palladium diacetate; triphenylphosphine / 1,2-dimethoxyethane; water / 4 h / 56 °C

2: tetrakis(actonitrile)copper(I) hexafluorophosphate; iodosylbenzene; ethylenediamine / acetonitrile / 48 h / 20 °C / Molecular sieve

With tetrakis(actonitrile)copper(I) hexafluorophosphate; barium hydroxide octahydrate; iodosylbenzene; palladium diacetate; ethylenediamine; triphenylphosphine; In 1,2-dimethoxyethane; water; acetonitrile; 1: Suzuki coupling;
DOI:10.1021/ol202436a