allyl 9-deoxy-9-oxo-α-apopicropodophyllate

Base Information

• Chemical Name: allyl 9-deoxy-9-oxo-α-apopicropodophyllate
• CAS No.: 1207260-87-4
• Molecular Formula: C₂₅H₂₄O₈
• Molecular Weight: 452.461

Synonyms:allyl 9-deoxy-9-oxo-α-apopicropodophyllate

Chemical Property of allyl 9-deoxy-9-oxo-α-apopicropodophyllate

Chemical Property:

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Technology Process of allyl 9-deoxy-9-oxo-α-apopicropodophyllate

There total 1 articles about allyl 9-deoxy-9-oxo-α-apopicropodophyllate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

allyl picropodophyllate (1207260-80-7) → allyl 9-deoxy-9-oxo-α-apopicropodophyllate (1207260-87-4)

Guidance literature:

allyl picropodophyllate; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -55 ℃; for 0.5h;

With triethylamine; In dichloromethane; at -55 - 0 ℃; for 1h;

DOI:10.1021/jm901373w

upstream raw materials:

allyl picropodophyllate

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