5'-O-(4,4'-dimethoxytrityl)-3'-S-acetyl-2'-O-methyl-N²-isobutyryl-3'-thioguanosine

Base Information

• Chemical Name: 5'-O-(4,4'-dimethoxytrityl)-3'-S-acetyl-2'-O-methyl-N²-isobutyryl-3'-thioguanosine
• CAS No.: 1042664-52-7
• Molecular Formula: C₃₈H₄₁N₅O₈S
• Molecular Weight: 727.838

Synonyms:5'-O-(4,4'-dimethoxytrityl)-3'-S-acetyl-2'-O-methyl-N²-isobutyryl-3'-thioguanosine

Chemical Property of 5'-O-(4,4'-dimethoxytrityl)-3'-S-acetyl-2'-O-methyl-N²-isobutyryl-3'-thioguanosine

Chemical Property:

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Technology Process of 5'-O-(4,4'-dimethoxytrityl)-3'-S-acetyl-2'-O-methyl-N²-isobutyryl-3'-thioguanosine

There total 1 articles about 5'-O-(4,4'-dimethoxytrityl)-3'-S-acetyl-2'-O-methyl-N²-isobutyryl-3'-thioguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

3'-S-acetyl-2'-O-methyl-N2-isobutyryl-3'-thioguanosine (1042664-51-6) + 4,4'-dimethoxytrityl chloride (40615-36-9) → 5'-O-(4,4'-dimethoxytrityl)-3'-S-acetyl-2'-O-methyl-N2-isobutyryl-3'-thioguanosine (1042664-52-7)

Guidance literature:

With pyridine; at 20 ℃; for 20h;

DOI:10.1016/j.bmc.2008.03.061

Reference yield: 85.0%

5'-O-(4,4'-dimethoxytrityl)-3'-S-acetyl-2'-O-methyl-N2-isobutyryl-3'-thioguanosine (1042664-52-7) → 5'-O-(4,4'-dimethoxytrityl)-2'-O-methyl-N2-isobutyryl-3'-thioguanosine (1042664-53-8)

Guidance literature:

With methanol; guanidine hydrochloride; sodium methylate; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1016/j.bmc.2008.03.061

upstream raw materials:

3'-S-acetyl-2'-O-methyl-N²-isobutyryl-3'-thioguanosine

4,4'-dimethoxytrityl chloride

Downstream raw materials:

5'-O-(4,4'-dimethoxytrityl)-2'-O-methyl-N²-isobutyryl-3'-thioguanosine

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