Technology Process of C38H26F6P2
There total 7 articles about C38H26F6P2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; trichlorosilane;
In
toluene;
at 0 ℃;
for 5h;
Inert atmosphere;
Reflux;
DOI:10.1246/bcsj.20110309
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: boron tribromide / dichloromethane / 3 h / -78 - 20 °C / Inert atmosphere
1.2: 0 °C
2.1: 2,6-dimethylpyridine / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere
3.1: 1,4-diaza-bicyclo[2.2.2]octane; 1,2-bis(diphenylphosphino)ethane nickel(II) chloride / N,N-dimethyl-formamide / 30 h / 100 °C / Inert atmosphere
4.1: dmap; trichlorosilane / toluene / 5 h / 0 °C / Inert atmosphere; Reflux
With
1,4-diaza-bicyclo[2.2.2]octane; 2,6-dimethylpyridine; dmap; 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; trichlorosilane; boron tribromide;
In
dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1246/bcsj.20110309
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2,6-dimethylpyridine / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere
2: 1,4-diaza-bicyclo[2.2.2]octane; 1,2-bis(diphenylphosphino)ethane nickel(II) chloride / N,N-dimethyl-formamide / 30 h / 100 °C / Inert atmosphere
3: dmap; trichlorosilane / toluene / 5 h / 0 °C / Inert atmosphere; Reflux
With
1,4-diaza-bicyclo[2.2.2]octane; 2,6-dimethylpyridine; dmap; 1,2-bis(diphenylphosphino)ethane nickel(II) chloride; trichlorosilane;
In
dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1246/bcsj.20110309