9-(5-O-benzoyl-2,3-dideoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)-6-hydroxy-2-isobutyramidopurin

Base Information

Chemical Name:9-(5-O-benzoyl-2,3-dideoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)-6-hydroxy-2-isobutyramidopurin
CAS No.:133272-10-3
Molecular Formula:C₂₆H₃₄N₅O₈P
Molecular Weight:575.558
Hs Code.:

Synonyms:9-(5-O-benzoyl-2,3-dideoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)-6-hydroxy-2-isobutyramidopurin

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Chemical Property of 9-(5-O-benzoyl-2,3-dideoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)-6-hydroxy-2-isobutyramidopurin

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Technology Process of 9-(5-O-benzoyl-2,3-dideoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)-6-hydroxy-2-isobutyramidopurin

There total 3 articles about 9-(5-O-benzoyl-2,3-dideoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)-6-hydroxy-2-isobutyramidopurin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 133272-09-0
9-(5-O-benzoyl-3-deoxy-3-diethoxyphosphorylmethyl-2-O-phenoxythiocarbonyl-β-D-ribofuranosyl)-6-hydroxy-2-isobutyramidopurin

: 133272-10-3
9-(5-O-benzoyl-2,3-dideoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)-6-hydroxy-2-isobutyramidopurin

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 70 ℃; for 2h;

Reference yield:

: 133294-70-9
9-(2-O-acetyl-5-O-benzoyl-3-deoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)-6-hydroxy-2-isobutyramidopurin

: 133272-10-3
9-(5-O-benzoyl-2,3-dideoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)-6-hydroxy-2-isobutyramidopurin

Guidance literature:: Multi-step reaction with 3 steps

1: 46 percent / hydroxylammonium acetate, pyridine / 66 h / Ambient temperature

2: 81 percent / 4-dimethylaminopyridine (DMAP) / 12 h / Ambient temperature

3: 67 percent / tributyltin hydride, azobisisobutyronitrile (AIBN) / toluene / 2 h / 70 °C

With pyridine; dmap; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; hydroxylamine acetate; In toluene;

Reference yield:

: 133272-08-9
9-(5-O-benzoyl-3-desoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)-6-hydroxy-2-isobutyramidopurin

: 133272-10-3
9-(5-O-benzoyl-2,3-dideoxy-3-diethoxyphosphorylmethyl-β-D-ribofuranosyl)-6-hydroxy-2-isobutyramidopurin

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / 4-dimethylaminopyridine (DMAP) / 12 h / Ambient temperature

2: 67 percent / tributyltin hydride, azobisisobutyronitrile (AIBN) / toluene / 2 h / 70 °C

With dmap; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene;