2,15-Bis-{(S)-2-hydroxy-1-[(R)-2-(2-methoxy-ethoxymethoxy)-2-phenyl-acetoxy]-propyl}-hexadecanedioic acid diisopropyl ester

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Chemical Name:2,15-Bis-{(S)-2-hydroxy-1-[(R)-2-(2-methoxy-ethoxymethoxy)-2-phenyl-acetoxy]-propyl}-hexadecanedioic acid diisopropyl ester
CAS No.:374538-63-3
Molecular Formula:C₅₂H₈₂O₁₆
Molecular Weight:963.213
Hs Code.:

Synonyms:2,15-Bis-{(S)-2-hydroxy-1-[(R)-2-(2-methoxy-ethoxymethoxy)-2-phenyl-acetoxy]-propyl}-hexadecanedioic acid diisopropyl ester

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Chemical Property of 2,15-Bis-{(S)-2-hydroxy-1-[(R)-2-(2-methoxy-ethoxymethoxy)-2-phenyl-acetoxy]-propyl}-hexadecanedioic acid diisopropyl ester

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Technology Process of 2,15-Bis-{(S)-2-hydroxy-1-[(R)-2-(2-methoxy-ethoxymethoxy)-2-phenyl-acetoxy]-propyl}-hexadecanedioic acid diisopropyl ester

There total 2 articles about 2,15-Bis-{(S)-2-hydroxy-1-[(R)-2-(2-methoxy-ethoxymethoxy)-2-phenyl-acetoxy]-propyl}-hexadecanedioic acid diisopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.4%

: 374538-61-1
2,15-Bis-{(S)-1-hydroxy-2-[(R)-2-(2-methoxy-ethoxymethoxy)-2-phenyl-acetoxy]-propyl}-hexadecanedioic acid diisopropyl ester

: 374538-63-3
2,15-Bis-{(S)-2-hydroxy-1-[(R)-2-(2-methoxy-ethoxymethoxy)-2-phenyl-acetoxy]-propyl}-hexadecanedioic acid diisopropyl ester

Guidance literature:: With sodium acetate; In N,N,N,N,N,N-hexamethylphosphoric triamide; N,N-dimethyl-formamide; at 50 ℃; for 5h;
DOI:10.1271/bbb.65.1903

Reference yield:

: 26720-45-6
Hexadecandisaeure-diisopropylester

: 374538-63-3
2,15-Bis-{(S)-2-hydroxy-1-[(R)-2-(2-methoxy-ethoxymethoxy)-2-phenyl-acetoxy]-propyl}-hexadecanedioic acid diisopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / LDA / tetrahydrofuran / 0.67 h / -78 °C

2: 44.4 percent / AcONa / dimethylformamide; hexamethylphosphoric acid triamide / 5 h / 50 °C

With sodium acetate; lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; N,N-dimethyl-formamide;
DOI:10.1271/bbb.65.1903