methyl 3-azido-2,3-dideoxy-5-O-triphenylmethyl-D-erythro-pentofuranoside

Base Information

Chemical Name:methyl 3-azido-2,3-dideoxy-5-O-triphenylmethyl-D-erythro-pentofuranoside
CAS No.:532413-72-2
Molecular Formula:C₂₅H₂₅N₃O₃
Molecular Weight:415.492
Hs Code.:

Synonyms:methyl 3-azido-2,3-dideoxy-5-O-triphenylmethyl-D-erythro-pentofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-azido-2,3-dideoxy-5-O-triphenylmethyl-D-erythro-pentofuranoside

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Technology Process of methyl 3-azido-2,3-dideoxy-5-O-triphenylmethyl-D-erythro-pentofuranoside

There total 8 articles about methyl 3-azido-2,3-dideoxy-5-O-triphenylmethyl-D-erythro-pentofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 116390-98-8
methyl 2-deoxy-3-O-methanesulfonyl-5-O-triphenylmethyl-β-D-threo-pentofuranoside

: 532413-72-2
methyl 3-azido-2,3-dideoxy-5-O-triphenylmethyl-D-erythro-pentofuranoside

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 110 ℃; for 2h;
DOI:10.1016/S0008-6215(02)00397-X

Reference yield:

: 116390-97-7,116390-98-8,138147-23-6,138147-24-7
Methanesulfonic acid (2R,3R)-5-methoxy-2-trityloxymethyl-tetrahydro-furan-3-yl ester

: 532413-72-2
methyl 3-azido-2,3-dideoxy-5-O-triphenylmethyl-D-erythro-pentofuranoside

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 100 ℃; Yield given;

Reference yield:

: Methanesulfonic acid (2R,3S,4R,5R)-5-methoxy-4-methylsulfanylthiocarboxyoxy-2-trityloxymethyl-tetrahydro-furan-3-yl ester

: 532413-72-2
methyl 3-azido-2,3-dideoxy-5-O-triphenylmethyl-D-erythro-pentofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / n-Bu₃SnH; AIBN / toluene / 2 h / Heating

2: 93 percent / sodium azide / dimethylformamide / 2 h / 110 °C

With sodium azide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/S0008-6215(02)00397-X