Cp₂Ti(SeC₆H₄Me-m)2

Base Information

• Chemical Name: Cp₂Ti(SeC₆H₄Me-m)2
• CAS No.: 727739-15-3
• Molecular Formula: C₂₄H₂₄Se₂Ti
• Molecular Weight: 518.255
• Mol file: 727739-15-3.mol

Synonyms:Cp₂Ti(SeC₆H₄Me-m)2

Chemical Property of Cp₂Ti(SeC₆H₄Me-m)2

Chemical Property:

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Technology Process of Cp₂Ti(SeC₆H₄Me-m)2

There total 1 articles about Cp₂Ti(SeC₆H₄Me-m)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

bis(cyclopentadienyl)titanium dichloride (1271-19-8) + bis(3-methylphenyl) diselenide (69468-42-4) → Cp2Ti(SeC6H4Me-m)2 (727739-15-3)

Guidance literature:

With Mg; 1,2-Br₂C₂H₄; In tetrahydrofuran; (Ar); a flask charged with Mg, THF, and 1,2-Br2C2H4, heated gently, Ti complex added, stirred at room temp., diselenide added, stirred at room temp.; evapd. (vac.), chromd. (CH2Cl2/petroleum ether), recrystd. (CH2Cl2/hexane); elem. anal.;

DOI:10.1016/j.ica.2003.06.011

upstream raw materials:

bis(cyclopentadienyl)titanium dichloride

bis(3-methylphenyl) diselenide