Cyclopropaneacetic acid, 2-[[(1,1-dimethylethoxy)carbonyl]amino]-, (1R,2S)-

Base Information

Chemical Name:Cyclopropaneacetic acid, 2-[[(1,1-dimethylethoxy)carbonyl]amino]-, (1R,2S)-
CAS No.:308266-57-1
Molecular Formula:C₁₀H₁₇NO₄
Molecular Weight:215.249
Hs Code.:
Mol file:308266-57-1.mol

Synonyms:Cyclopropaneacetic acid, 2-[[(1,1-dimethylethoxy)carbonyl]amino]-, (1R,2S)-

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Chemical Property of Cyclopropaneacetic acid, 2-[[(1,1-dimethylethoxy)carbonyl]amino]-, (1R,2S)-

Chemical Property:

Boiling Point:373.1±11.0 °C(Predicted)
PKA:4.76±0.10(Predicted)
PSA：0.00000
Density:1.17±0.1 g/cm3(Predicted)
LogP:0.00000

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Cyclopropaneacetic acid, 2-[[(1,1-dimethylethoxy)carbonyl]amino]-, (1R,2S)-

There total 30 articles about Cyclopropaneacetic acid, 2-[[(1,1-dimethylethoxy)carbonyl]amino]-, (1R,2S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 171550-09-7
tert-butyl [(1R,2S)-2-(2-hydroxyethyl)cyclopropyl]carbamate

: 308266-57-1
(1S,2R)-2-(t-buthoxycarbonyl)amino-1-(carboxymethyl)cyclopropane

Guidance literature:: tert-butyl [(1R,2S)-2-(2-hydroxyethyl)cyclopropyl]carbamate; With Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃; for 2h;

With sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; In water; tert-butyl alcohol; at 20 ℃; for 1h;
DOI:10.1016/j.bmc.2013.06.063

Reference yield: 64.0%

: 171550-09-7
tert-butyl [(Z)-(2-hydroxyethyl)cyclopropyl]carbamate

: 308266-57-1
2-{(Z)-[(tert-butoxycarbonyl)amino]cyclopropyl}acetic acid

Guidance literature:: With potassium permanganate; sodium hydroxide; In water; tert-butyl alcohol; at 20 ℃; for 16h; Darkness; Inert atmosphere;
DOI:10.1039/c1ob06095c

Reference yield: 55.0%

: 1338807-58-1,171550-09-7
tert-butyl [(1S,2R)-2-(2-hydroxyethyl)cyclopropyl]carbamate

: 1338807-60-5,308266-57-1
(1R,2S)-trans-2-(t-buthoxycarbonyl)amino-1-(carboxymethyl)cyclopropane

Guidance literature:: With potassium permanganate; sodium hydroxide; In water; tert-butyl alcohol; at 20 ℃; for 16h; Darkness; Inert atmosphere;
DOI:10.1039/c1ob06095c