2,3-bis(3,4-dibutoxyphenyl)quinoxaline-6-carboxylic acid 4-(6-dodecyloxy benzoxazol-2-yl)phenyl ester

Base Information

Chemical Name:2,3-bis(3,4-dibutoxyphenyl)quinoxaline-6-carboxylic acid 4-(6-dodecyloxy benzoxazol-2-yl)phenyl ester
CAS No.:1262970-28-4
Molecular Formula:C₆₂H₇₇N₃O₈
Molecular Weight:992.309
Hs Code.:

Synonyms:2,3-bis(3,4-dibutoxyphenyl)quinoxaline-6-carboxylic acid 4-(6-dodecyloxy benzoxazol-2-yl)phenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-bis(3,4-dibutoxyphenyl)quinoxaline-6-carboxylic acid 4-(6-dodecyloxy benzoxazol-2-yl)phenyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2,3-bis(3,4-dibutoxyphenyl)quinoxaline-6-carboxylic acid 4-(6-dodecyloxy benzoxazol-2-yl)phenyl ester

There total 7 articles about 2,3-bis(3,4-dibutoxyphenyl)quinoxaline-6-carboxylic acid 4-(6-dodecyloxy benzoxazol-2-yl)phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2,3-bis(3,4-dibutyloxyphenyl)quinoxaline-6-carboxylic acid 4-[(4-dodecyloxy-2-hydroxyphenylimino)methyl]phenyl ester

: 1262970-28-4
2,3-bis(3,4-dibutoxyphenyl)quinoxaline-6-carboxylic acid 4-(6-dodecyloxy benzoxazol-2-yl)phenyl ester

Guidance literature:: With lead(IV) tetraacetate; In chloroform; for 2h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2010.11.014

Reference yield:

: 656811-18-6
5-dodecyloxy-2-nitrophenol

: 1262970-28-4
2,3-bis(3,4-dibutoxyphenyl)quinoxaline-6-carboxylic acid 4-(6-dodecyloxy benzoxazol-2-yl)phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 10% palladium on activated carbon; hydrazine / ethanol / 24 h / Reflux

2: ethanol / 3 h / Reflux

3: lead(IV) tetraacetate / chloroform / 2 h / Inert atmosphere; Reflux

With 10% palladium on activated carbon; lead(IV) tetraacetate; hydrazine; In ethanol; chloroform;
DOI:10.1016/j.tet.2010.11.014

Reference yield:

: C₃₇H₄₆N₂O₆

: 1262970-28-4
2,3-bis(3,4-dibutoxyphenyl)quinoxaline-6-carboxylic acid 4-(6-dodecyloxy benzoxazol-2-yl)phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C

2: ethanol / 3 h / Reflux

3: lead(IV) tetraacetate / chloroform / 2 h / Inert atmosphere; Reflux

With dmap; lead(IV) tetraacetate; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1016/j.tet.2010.11.014