3-(4-Bromo-phenyl)-2-cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-thiopropionamide; compound with morpholine

Base Information

• Chemical Name: 3-(4-Bromo-phenyl)-2-cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-thiopropionamide; compound with morpholine
• CAS No.: 131270-69-4
• Molecular Formula: C₄H₉NO*C₁₈H₁₉BrN₂O₂S
• Molecular Weight: 494.453

Synonyms:3-(4-Bromo-phenyl)-2-cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-thiopropionamide; compound with morpholine

Chemical Property of 3-(4-Bromo-phenyl)-2-cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-thiopropionamide; compound with morpholine

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Technology Process of 3-(4-Bromo-phenyl)-2-cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-thiopropionamide; compound with morpholine

There total 6 articles about 3-(4-Bromo-phenyl)-2-cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-thiopropionamide; compound with morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

morpholine (110-91-8,99108-56-2) + 3-(4-bromophenyl)-2-cyanoprop-2-enethioamide (68029-54-9,95639-00-2) + dimedone (126-81-8) → 3-(4-Bromo-phenyl)-2-cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-thiopropionamide; compound with morpholine (131270-69-4)

Guidance literature:

In ethanol; at 20 - 25 ℃; for 5h;

Reference yield: 91.0%

morpholine (110-91-8,99108-56-2) + (E)-3-(4-bromophenyl)-2-cyanoprop-2-enethioamide (68029-54-9) + dimedone (126-81-8) → 3-(4-Bromo-phenyl)-2-cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-thiopropionamide; compound with morpholine (131270-69-4)

Guidance literature:

In ethanol; at 25 ℃; for 5h;

Reference yield: 69.0%

morpholine (110-91-8,99108-56-2) + 2-amino-4-(4-bromophenyl)-7,7-dimethyl-5-oxo-3-thiocarbamoyl-5,6,7,8-tetrahydro-4H-benzopyran (117822-66-9) → 3-(4-Bromo-phenyl)-2-cyano-3-(2-hydroxy-4,4-dimethyl-6-oxo-cyclohex-1-enyl)-thiopropionamide; compound with morpholine (131270-69-4)

Guidance literature:

In ethanol; at 25 ℃; for 5h;

upstream raw materials:

morpholine

2-amino-4-(4-bromophenyl)-7,7-dimethyl-5-oxo-3-thiocarbamoyl-5,6,7,8-tetrahydro-4H-benzopyran

3-(4-bromophenyl)-2-cyanoprop-2-enethioamide

dimedone

Downstream raw materials:

4-(4-bromophenyl)-7,7-dimethyl-5-oxo-3-cyano-3,4,5,6,7,8-hexahydro-2(1H)-quinolinethione

3-(5,5-dimethyl-1-hydroxy-3-oxo-1-cyclohexen-2-yl)-3-(4-bromophenyl)-2-cyanopropanecarbothioamide

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