benzyl 3-((tert-butoxycarbonyl)amino)-3-(hydroxymethyl)pyrrolidine-1-carboxylate

Base Information

Chemical Name:benzyl 3-((tert-butoxycarbonyl)amino)-3-(hydroxymethyl)pyrrolidine-1-carboxylate
CAS No.:1004992-31-7
Molecular Formula:C₁₈H₂₆N₂O₅
Molecular Weight:350.415
Hs Code.:

Synonyms:benzyl 3-((tert-butoxycarbonyl)amino)-3-(hydroxymethyl)pyrrolidine-1-carboxylate

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Chemical Property of benzyl 3-((tert-butoxycarbonyl)amino)-3-(hydroxymethyl)pyrrolidine-1-carboxylate

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Technology Process of benzyl 3-((tert-butoxycarbonyl)amino)-3-(hydroxymethyl)pyrrolidine-1-carboxylate

There total 2 articles about benzyl 3-((tert-butoxycarbonyl)amino)-3-(hydroxymethyl)pyrrolidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 675834-18-1
1-benzyl 3-methyl 3-((tert-butoxycarbonyl)amino)pyrrolidine-1,3-dicarboxylate

: 1004992-31-7
benzyl 3-((tert-butoxycarbonyl)amino)-3-(hydroxymethyl)pyrrolidine-1-carboxylate

Guidance literature:: 1-benzyl 3-methyl 3-((tert-butoxycarbonyl)amino)pyrrolidine-1,3-dicarboxylate; With 4-methyl-morpholine; chloroformic acid ethyl ester; In tetrahydrofuran; at 0 ℃; for 0.166667h;

With sodium tetrahydroborate; In water; at 0 ℃; for 0.5h;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 475469-15-9
(3-hydroxymethyl-pyrrolidin-3-yl)-carbamic acid tert-butyl ester

: 1004992-31-7
benzyl 3-((tert-butoxycarbonyl)amino)-3-(hydroxymethyl)pyrrolidine-1-carboxylate

Guidance literature:: With triethylamine; In dichloromethane; at -60 - 25 ℃;

Reference yield: 94.0%

: 1004992-31-7
benzyl 3-((tert-butoxycarbonyl)amino)-3-(hydroxymethyl)pyrrolidine-1-carboxylate

: 1004992-32-8
C₁₈H₂₄N₂O₆S

Guidance literature:: benzyl 3-((tert-butoxycarbonyl)amino)-3-(hydroxymethyl)pyrrolidine-1-carboxylate; With thionyl chloride; In acetonitrile; at -40 ℃;

With pyridine; In acetonitrile; at 25 ℃; for 0.583333h;