2-cyano-N'-(2-oxoindolin-3-ylidene)-3-(phenylamino)-3-thioxopropanehydrazide

Base Information

Chemical Name:2-cyano-N'-(2-oxoindolin-3-ylidene)-3-(phenylamino)-3-thioxopropanehydrazide
CAS No.:1431861-28-7
Molecular Formula:C₁₈H₁₃N₅O₂S
Molecular Weight:363.4
Hs Code.:

Synonyms:2-cyano-N'-(2-oxoindolin-3-ylidene)-3-(phenylamino)-3-thioxopropanehydrazide

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Chemical Property of 2-cyano-N'-(2-oxoindolin-3-ylidene)-3-(phenylamino)-3-thioxopropanehydrazide

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Technology Process of 2-cyano-N'-(2-oxoindolin-3-ylidene)-3-(phenylamino)-3-thioxopropanehydrazide

There total 2 articles about 2-cyano-N'-(2-oxoindolin-3-ylidene)-3-(phenylamino)-3-thioxopropanehydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 29775-72-2
2-cyano-N'-(2-oxo-1,2-dihydroindol-3-ylidene)acetohydrazide

: 103-72-0
phenyl isothiocyanate

: 1431861-28-7
2-cyano-N'-(2-oxoindolin-3-ylidene)-3-(phenylamino)-3-thioxopropanehydrazide

Guidance literature:: 2-cyano-N'-(2-oxo-1,2-dihydroindol-3-ylidene)acetohydrazide; With potassium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

phenyl isothiocyanate; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

With hydrogenchloride; In water; N,N-dimethyl-formamide;
DOI:10.3184/174751912X13567100793191

Reference yield:

: 91-56-5,1186480-61-4,84788-92-1
indole-2,3-dione

: 1431861-28-7
2-cyano-N'-(2-oxoindolin-3-ylidene)-3-(phenylamino)-3-thioxopropanehydrazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,4-dioxane / 0.08 h / Reflux

2.1: potassium hydroxide / N,N-dimethyl-formamide / 0.5 h / 20 °C

2.2: 12 h / 20 °C

With potassium hydroxide; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.3184/174751912X13567100793191