N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-N₆-methyl-1,3,5-triazine-2,4,6-triamine

Base Information

Chemical Name:N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-N₆-methyl-1,3,5-triazine-2,4,6-triamine
CAS No.:1352803-87-2
Molecular Formula:C₂₅H₃₃N₇
Molecular Weight:431.584
Hs Code.:

N<sub>2</sub>-(1-benzylpiperidin-4-yl)-N<sub>4</sub>-mesityl-N<sub>6</sub>-methyl-1,3,5-triazine-2,4,6-triamine

Synonyms:N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-N₆-methyl-1,3,5-triazine-2,4,6-triamine

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Chemical Property of N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-N₆-methyl-1,3,5-triazine-2,4,6-triamine

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Technology Process of N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-N₆-methyl-1,3,5-triazine-2,4,6-triamine

There total 3 articles about N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-N₆-methyl-1,3,5-triazine-2,4,6-triamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.6%

: 1352804-11-5
N₂-mesityl-N₄-methyl-N₆-(piperidin-4-yl)-1,3,5-triazine-2,4,6-triamine

: 1352803-87-2
N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-N₆-methyl-1,3,5-triazine-2,4,6-triamine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1016/j.ejmech.2012.02.019

Reference yield:

: 1352804-07-9
6-chloro-N₂-mesityl-N₄-(1-Boc-piperidin-4-yl)-1,3,5-triazine-2,4-diamine

: 1352803-87-2
N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-N₆-methyl-1,3,5-triazine-2,4,6-triamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate / tetrahydrofuran; water / 5 h / 50 °C

2.1: trifluoroacetic acid / dichloromethane / 20 °C

2.2: pH 8

3.1: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C

With sodium hydrogencarbonate; potassium carbonate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.02.019

Reference yield:

: 4,6-dichloro-N-mesityl-1,3,5-triazin-2-amine

: 1352803-87-2
N₂-(1-benzylpiperidin-4-yl)-N₄-mesityl-N₆-methyl-1,3,5-triazine-2,4,6-triamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate / tetrahydrofuran; water; acetone / 8 h / 30 °C

2.1: sodium hydrogencarbonate / tetrahydrofuran; water / 5 h / 50 °C

3.1: trifluoroacetic acid / dichloromethane / 20 °C

3.2: pH 8

4.1: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C

With sodium hydrogencarbonate; potassium carbonate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.ejmech.2012.02.019