Technology Process of C10H4ClF6N3S
There total 4 articles about C10H4ClF6N3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sulfur dichloride;
In
acetonitrile;
Reflux;
Inert atmosphere;
DOI:10.1021/ic2003996
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride / diethyl ether / Inert atmosphere
2: sulfur dichloride / acetonitrile / Reflux; Inert atmosphere
With
hydrogenchloride; sulfur dichloride;
In
diethyl ether; acetonitrile;
DOI:10.1021/ic2003996
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium bis(trimethylsilyl)amide diethyl etherate / diethyl ether / Inert atmosphere
1.2: Inert atmosphere
1.3: Inert atmosphere
2.1: acetonitrile / -196 - 60 °C / Inert atmosphere
3.1: hydrogenchloride / diethyl ether / Inert atmosphere
4.1: sulfur dichloride / acetonitrile / Reflux; Inert atmosphere
With
hydrogenchloride; sulfur dichloride; lithium bis(trimethylsilyl)amide diethyl etherate;
In
diethyl ether; acetonitrile;
DOI:10.1021/ic2003996