(S)-2-(3-(2-amino-3-(4-chlorophenyl)propanamido)-5-(pyridin-4-yl)phenyl)-2-methylpropanoic acid trifluoroacetic acid salt

Base Information

Chemical Name:(S)-2-(3-(2-amino-3-(4-chlorophenyl)propanamido)-5-(pyridin-4-yl)phenyl)-2-methylpropanoic acid trifluoroacetic acid salt
CAS No.:1240524-39-3
Molecular Formula:C₂HF₃O₂*C₂₄H₂₄ClN₃O₃
Molecular Weight:551.95
Hs Code.:

Synonyms:(S)-2-(3-(2-amino-3-(4-chlorophenyl)propanamido)-5-(pyridin-4-yl)phenyl)-2-methylpropanoic acid trifluoroacetic acid salt

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Chemical Property of (S)-2-(3-(2-amino-3-(4-chlorophenyl)propanamido)-5-(pyridin-4-yl)phenyl)-2-methylpropanoic acid trifluoroacetic acid salt

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Technology Process of (S)-2-(3-(2-amino-3-(4-chlorophenyl)propanamido)-5-(pyridin-4-yl)phenyl)-2-methylpropanoic acid trifluoroacetic acid salt

There total 3 articles about (S)-2-(3-(2-amino-3-(4-chlorophenyl)propanamido)-5-(pyridin-4-yl)phenyl)-2-methylpropanoic acid trifluoroacetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₄₀ClN₃O₅

: 76-05-1
trifluoroacetic acid

: 1240524-39-3
(S)-2-(3-(2-amino-3-(4-chlorophenyl)propanamido)-5-(pyridin-4-yl)phenyl)-2-methylpropanoic acid trifluoroacetic acid salt

Guidance literature:: In dichloromethane; at 20 ℃; for 4h;

Reference yield:

: 1240524-36-0
tert-butyl 2-methyl-2-(3-nitro-5-(pyridin-4-yl)phenyl)propanoate

: 1240524-39-3
(S)-2-(3-(2-amino-3-(4-chlorophenyl)propanamido)-5-(pyridin-4-yl)phenyl)-2-methylpropanoic acid trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 6 h / 20 °C

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 6 h / 50 °C

3: dichloromethane / 4 h / 20 °C

With hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; palladium 10% on activated carbon; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1240524-37-1
tert-butyl 2-(3-amino-5-(pyridin-4-yl)phenyl)-2-methylpropanoate

: 1240524-39-3
(S)-2-(3-(2-amino-3-(4-chlorophenyl)propanamido)-5-(pyridin-4-yl)phenyl)-2-methylpropanoic acid trifluoroacetic acid salt

Guidance literature:: Multi-step reaction with 2 steps

1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 6 h / 50 °C

2: dichloromethane / 4 h / 20 °C

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;