1,1'-[3,3'-disulfanediylbis(propane-3,1-diyl)]bis(3-ethyl-4-phenyl-1H-pyrrole-2,5-dione)

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Chemical Name:1,1'-[3,3'-disulfanediylbis(propane-3,1-diyl)]bis(3-ethyl-4-phenyl-1H-pyrrole-2,5-dione)
CAS No.:1384256-57-8
Molecular Formula:C₃₀H₃₂N₂O₄S₂
Molecular Weight:548.727
Hs Code.:

Synonyms:1,1'-[3,3'-disulfanediylbis(propane-3,1-diyl)]bis(3-ethyl-4-phenyl-1H-pyrrole-2,5-dione)

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Chemical Property of 1,1'-[3,3'-disulfanediylbis(propane-3,1-diyl)]bis(3-ethyl-4-phenyl-1H-pyrrole-2,5-dione)

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Technology Process of 1,1'-[3,3'-disulfanediylbis(propane-3,1-diyl)]bis(3-ethyl-4-phenyl-1H-pyrrole-2,5-dione)

There total 4 articles about 1,1'-[3,3'-disulfanediylbis(propane-3,1-diyl)]bis(3-ethyl-4-phenyl-1H-pyrrole-2,5-dione) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 1384256-37-4
(Z)-3-(2,2-dichlorobutanoyl)-2-benzylidene-1,3-thiazinane

: 1384256-58-9
3-ethyl-1-{3-(7-ethyl-6-oxo-8-phenyl-3,4,6,8a-tetrahydro-2H-pyrrolo[2,1-b]-1,3-thiazin-8a-ylthio)propyl}-4-phenyl-1H-pyrrole-2,5-dione

: 1384256-57-8
1,1'-[3,3'-disulfanediylbis(propane-3,1-diyl)]bis(3-ethyl-4-phenyl-1H-pyrrole-2,5-dione)

Guidance literature:: (Z)-3-(2,2-dichlorobutanoyl)-2-benzylidene-1,3-thiazinane; With N,N,N,N,-tetramethylethylenediamine; sodium carbonate; copper(l) chloride; In acetonitrile; at 30 ℃; for 17h; Inert atmosphere;

With water; In acetonitrile; Inert atmosphere;
DOI:10.1016/j.tet.2012.04.117

Reference yield:

: 124932-16-7
N-(3-hydroxypropyl)-2-phenylacetamide

: 1384256-58-9
3-ethyl-1-{3-(7-ethyl-6-oxo-8-phenyl-3,4,6,8a-tetrahydro-2H-pyrrolo[2,1-b]-1,3-thiazin-8a-ylthio)propyl}-4-phenyl-1H-pyrrole-2,5-dione

: 1384256-57-8
1,1'-[3,3'-disulfanediylbis(propane-3,1-diyl)]bis(3-ethyl-4-phenyl-1H-pyrrole-2,5-dione)

Guidance literature:: Multi-step reaction with 3 steps

1.1: Lawessons reagent / toluene / 1.5 h / 120 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 18 h / 20 °C

3.1: N,N,N,N,-tetramethylethylenediamine; sodium carbonate; copper(l) chloride / acetonitrile / 17 h / 30 °C / Inert atmosphere

3.2: Inert atmosphere

With Lawessons reagent; N,N,N,N,-tetramethylethylenediamine; sodium carbonate; triethylamine; copper(l) chloride; In dichloromethane; toluene; acetonitrile;
DOI:10.1016/j.tet.2012.04.117

Reference yield:

: 25478-53-9
5,6-dihydro-2-benzyl-4H-1,3-thiazine

: 1384256-58-9
3-ethyl-1-{3-(7-ethyl-6-oxo-8-phenyl-3,4,6,8a-tetrahydro-2H-pyrrolo[2,1-b]-1,3-thiazin-8a-ylthio)propyl}-4-phenyl-1H-pyrrole-2,5-dione

: 1384256-57-8
1,1'-[3,3'-disulfanediylbis(propane-3,1-diyl)]bis(3-ethyl-4-phenyl-1H-pyrrole-2,5-dione)

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 18 h / 20 °C

2.1: N,N,N,N,-tetramethylethylenediamine; sodium carbonate; copper(l) chloride / acetonitrile / 17 h / 30 °C / Inert atmosphere

2.2: Inert atmosphere

With N,N,N,N,-tetramethylethylenediamine; sodium carbonate; triethylamine; copper(l) chloride; In dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2012.04.117