triisopropyl[(5Z,7E)-(5-⁽¹³⁾C)4-methanesulfonyl-8-phenyl-4-azaocta-5,7-dien-1-yn-6-yloxy]silane

Base Information

• Chemical Name: triisopropyl[(5Z,7E)-(5-⁽¹³⁾C)4-methanesulfonyl-8-phenyl-4-azaocta-5,7-dien-1-yn-6-yloxy]silane
• CAS No.: 1005482-00-7
• Molecular Formula: C₂₃H₃₅NO₃SSi
• Molecular Weight: 434.676

Synonyms:triisopropyl[(5Z,7E)-(5-⁽¹³⁾C)4-methanesulfonyl-8-phenyl-4-azaocta-5,7-dien-1-yn-6-yloxy]silane

Chemical Property of triisopropyl[(5Z,7E)-(5-⁽¹³⁾C)4-methanesulfonyl-8-phenyl-4-azaocta-5,7-dien-1-yn-6-yloxy]silane

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Technology Process of triisopropyl[(5Z,7E)-(5-⁽¹³⁾C)4-methanesulfonyl-8-phenyl-4-azaocta-5,7-dien-1-yn-6-yloxy]silane

There total 1 articles about triisopropyl[(5Z,7E)-(5-⁽¹³⁾C)4-methanesulfonyl-8-phenyl-4-azaocta-5,7-dien-1-yn-6-yloxy]silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

(E)-(4-(13)C)5-methanesulfonyl-1-phenyl-5-azaoct-1-en-7-yn-3-one (1005481-99-1) + triisopropylsilyl trifluoromethanesulfonate (80522-42-5) → triisopropyl[(5Z,7E)-(5-(13)C)4-methanesulfonyl-8-phenyl-4-azaocta-5,7-dien-1-yn-6-yloxy]silane (1005482-00-7)

Guidance literature:

With triethylamine; In dichloromethane;

DOI:10.1021/ja0782605

Reference yield: 86.0%

triisopropyl[(5Z,7E)-(5-(13)C)4-methanesulfonyl-8-phenyl-4-azaocta-5,7-dien-1-yn-6-yloxy]silane (1005482-00-7) → (5RS,6SR)-2-(13)C8-triisopropylsiloxy-3-methanesulfonyl-6-phenyl-3-azabicyclo[3.3.0]octa-1,7-diene

Guidance literature:

With 4 A molecular sieve; tungsten hexacarbonyl; tributyl-amine; In toluene; UV-irradiation;

DOI:10.1021/ja0782605

upstream raw materials:

(E)-(4-⁽¹³⁾C)5-methanesulfonyl-1-phenyl-5-azaoct-1-en-7-yn-3-one

triisopropylsilyl trifluoromethanesulfonate

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