(E)-3-(1-{4-[3-(2-pyridin-2-ylvinyl)phenylamino]phenyl}-1H-[1,2,3]triazol-4-yl)propan-1-ol

Base Information

Chemical Name:(E)-3-(1-{4-[3-(2-pyridin-2-ylvinyl)phenylamino]phenyl}-1H-[1,2,3]triazol-4-yl)propan-1-ol
CAS No.:1401773-94-1
Molecular Formula:C₂₄H₂₃N₅O
Molecular Weight:397.48
Hs Code.:

Synonyms:(E)-3-(1-{4-[3-(2-pyridin-2-ylvinyl)phenylamino]phenyl}-1H-[1,2,3]triazol-4-yl)propan-1-ol

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Chemical Property of (E)-3-(1-{4-[3-(2-pyridin-2-ylvinyl)phenylamino]phenyl}-1H-[1,2,3]triazol-4-yl)propan-1-ol

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Technology Process of (E)-3-(1-{4-[3-(2-pyridin-2-ylvinyl)phenylamino]phenyl}-1H-[1,2,3]triazol-4-yl)propan-1-ol

There total 6 articles about (E)-3-(1-{4-[3-(2-pyridin-2-ylvinyl)phenylamino]phenyl}-1H-[1,2,3]triazol-4-yl)propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1401774-24-0
4-bromo-(4-(3-hydroxypropyl)-1H-1,2,3-triazol-1-yl)benzene

: 176034-12-1
3-(trans-2-[2]pyridyl-vinyl)-aniline

: 1401773-94-1
(E)-3-(1-{4-[3-(2-pyridin-2-ylvinyl)phenylamino]phenyl}-1H-[1,2,3]triazol-4-yl)propan-1-ol

Guidance literature:: With potassium carbonate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos; In tert-butyl alcohol; at 90 ℃; for 20h; Inert atmosphere;

Reference yield: 44.0%

: 5390-04-5
pent-1-yn-5-ol

: 589-87-7
1,4-bromoiodobenzene

: 1379771-11-5
N-[2-(1-methoxybut-3-ynyl)phenyl]-4-nitrobenzenesulfonamide

: (4-(tert-butyl)-2,6-dimethylphenyl)boronic acid

: 589-87-7
1,4-bromoiodobenzene

: 1160930-69-7
5-(4-bromophenyl)-[2,2']bithiophene

: C₆₄H₄₄N₂

: 1373131-54-4
2-methyl-N-(2-methylphenyl)-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]benzenamine

: 1383003-87-9
4'-bromo-4-tert-butyl-2,6-dimethyl-1,1'-biphenyl

: 1401773-94-1
(E)-3-(1-{4-[3-(2-pyridin-2-ylvinyl)phenylamino]phenyl}-1H-[1,2,3]triazol-4-yl)propan-1-ol

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; for 5h; Inert atmosphere;
DOI:10.1021/ja303641p

Reference yield: 3.0%

: 5390-04-5
pent-1-yn-5-ol

: 589-87-7
1,4-bromoiodobenzene

: 1379771-11-5
N-[2-(1-methoxybut-3-ynyl)phenyl]-4-nitrobenzenesulfonamide

: (4-(tert-butyl)-2,6-dimethylphenyl)boronic acid

: 589-87-7
1,4-bromoiodobenzene

: 1160930-69-7
5-(4-bromophenyl)-[2,2']bithiophene

: C₆₄H₄₄N₂

: 1373131-54-4
2-methyl-N-(2-methylphenyl)-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]benzenamine

: 1383003-87-9
4'-bromo-4-tert-butyl-2,6-dimethyl-1,1'-biphenyl

: 1401773-94-1
(E)-3-(1-{4-[3-(2-pyridin-2-ylvinyl)phenylamino]phenyl}-1H-[1,2,3]triazol-4-yl)propan-1-ol

: C₂₃H₁₉BrN₂O₅S

Guidance literature:: 1,4-bromoiodobenzene; 4-(1-pyrrolidinyl)piperidine; With sodium t-butanolate; ruphos; In tetrahydrofuran; at 120 ℃; for 0.166667h; Inert atmosphere; Microwave irradiation;

trifluoroacetic acid; In tetrahydrofuran; at 20 ℃;
DOI:10.1039/c3md00197k