[1-(3,5-Bis-trifluoromethyl-phenyl)-eth-(E)-ylidene]-((S)-1-phenyl-ethyl)-amine

Base Information

Chemical Name:[1-(3,5-Bis-trifluoromethyl-phenyl)-eth-(E)-ylidene]-((S)-1-phenyl-ethyl)-amine
CAS No.:672906-98-8
Molecular Formula:C₁₈H₁₅F₆N
Molecular Weight:359.314
Hs Code.:

Synonyms:[1-(3,5-Bis-trifluoromethyl-phenyl)-eth-(E)-ylidene]-((S)-1-phenyl-ethyl)-amine

Suppliers and Price of [1-(3,5-Bis-trifluoromethyl-phenyl)-eth-(E)-ylidene]-((S)-1-phenyl-ethyl)-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [1-(3,5-Bis-trifluoromethyl-phenyl)-eth-(E)-ylidene]-((S)-1-phenyl-ethyl)-amine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of [1-(3,5-Bis-trifluoromethyl-phenyl)-eth-(E)-ylidene]-((S)-1-phenyl-ethyl)-amine

There total 1 articles about [1-(3,5-Bis-trifluoromethyl-phenyl)-eth-(E)-ylidene]-((S)-1-phenyl-ethyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2627-86-3
(S)-1-phenyl-ethylamine

: 30071-93-3
3,5-bis(trifluoromethyl)phenyl methyl ketone

: 672906-98-8
[1-(3,5-Bis-trifluoromethyl-phenyl)-eth-(E)-ylidene]-((S)-1-phenyl-ethyl)-amine

Guidance literature:: (S)-1-phenyl-ethylamine; 3,5-bis(trifluoromethyl)phenyl methyl ketone; With toluene-4-sulfonic acid; In toluene; for 24h; Heating / reflux;

With sodium hydrogencarbonate; In water;

Reference yield:

: 672906-98-8
[1-(3,5-Bis-trifluoromethyl-phenyl)-eth-(E)-ylidene]-((S)-1-phenyl-ethyl)-amine

: 384824-41-3
[(S)-1-(3,5-Bis-trifluoromethyl-phenyl)-ethyl]-((S)-1-phenyl-ethyl)-amine

: 511256-29-4
[(R)-1-(3,5-Bis-trifluoromethyl-phenyl)-ethyl]-((S)-1-phenyl-ethyl)-amine

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 12h;
DOI:10.1021/ol034014w

Reference yield:

: 672906-98-8
[1-(3,5-Bis-trifluoromethyl-phenyl)-eth-(E)-ylidene]-((S)-1-phenyl-ethyl)-amine

: 127733-40-8
(S)-α-(3,5-bis(trifluoromethyl)phenyl)ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium borohydride / methanol / 12 h / 0 °C

2: 98 percent / hydrogen; water / 5 percent Pd/C NX-type / methanol / 12 h / 60 °C / 3750.3 Torr

With sodium tetrahydroborate; water; hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1021/ol034014w